Weight of the fibrous part of H. B. (in uncertain-Greg hand)
Tbd to the Letter
H
We took two
[ 'several' deleted] ounces of the Fibrous part of Human Blood,
carefully separated from the Serum, & dry'd them
severally in 2 clear cak'd Glasses, the one in a South Window in the room over
our Laboratory, & the other
[ 'on the top' deleted] upon the Sand of our digestive furnace in a
part remote from the Focus where the Heat is alwayes very gentle.
The['se' at end of word deleted]
[ 'two parcels' deleted] former when it was dry enough to be
<easily> pulverable, weighed {drachm} iii + 5 g. & the latter {drachm} ii +
43 gr.
[Retrospective marginalia:]
2
{calx} of oyster shells (in uncertain-Greg hand)
Oyster shells free'd from their external scurf, were by being kept
above two hours
<in the fire> reduc'd (after some blackness) to a pure white
Calx, which discover'd it self to be much of the
nature of common Lime, not only by the Tast, but
[ 'fi' deleted] by these Marks 1. The powder of it being rub'd with Syrup
of Violets soon turn'd the Liquor green. 2. Some of the same Powder being
strow'd upon a Solution of Sublimate, presently afforded an Orange
Precipitate.
[Retrospective marginalia:]
3
[ 'fixation' deleted] odde {caput mortuum} fixt. (in uncertain-Greg hand)
Two half pounds of Oyl of Dantsic Vitriol, having been distill'd at
two several times with an equal weight of Spirits totally Ardent, afforded
about {ounce} ii of a cole-black Caput mortuum, which being put into a Crucible & kept
an hour in the fire, wasted to
<somewhat less than> half an ounce.
[space of 1/4 of page]
[Retrospective marginalia:]
4
Tb'd
{circle}
h (margin, at end of paragraph)
We took about the bigness of a walnut of clean cotton, & having
moisten'd it throughly with Chymical
[ '(' deleted] or (as Artists call it) Essential
[ ')' deleted] Oyl of Carvi, & then a little press'd it together, we
put it into a clean Copper Spoon, (because we had one at hand, & would
avoid spoiling a [BP 21, p. 220] Silver one) & then put to it a
little
[ 'of our the Liquor' deleted] very strong & smoking Vitriolic Spirit
of Nitre, made after our way, These Ingredients presently began to act on one
another, & the Cotton to grow black, & to emit
a['n' at end of word deleted] very thick
Smoke, which was in a trice follow'd by
<a large>[replacing 'an'] actual Flame,
[ 'very' deleted] as shining at least as that of a Candle, & somewhat
more yellow;
<
[ '(' deleted]Save that in one or two places it was of a fine blew, upon
the account, as I suppose of some corroded
[ 'C' deleted] Particles of the Copper Spoon
[ ')' deleted] >[insertion in margin ] It was accompany'd with Smoke, issuing out at the
top, as Flames usually are, &
[ 'being turn' deleted] being blown out,
<soon> rekindled of it self. § But this Tryal having been
made,
[ 'so near the fire' deleted] because
<
it 'twas>[replacing 'of the']
cold['ness' at end of word deleted]
Weather, so near the fire, that some of the Fumes that issu'd from the Mixture
before the Flame broke forth, might by a Sceptic be pretended to have been
kindl'd thereby, & so the fire be propagated to the Spoon; we repeated the
Experiment, in
[ 'an' deleted] another place (having divers Spoons at hand) & found,
as we expected, that it succeeded as before;
[ '&' deleted] save that, because Tryal was
<well &> carefully made, the success was somewhat better;
for the Flame being blown out three or 4 several times, was spontaneously
rekindl'd, & the Cotton burnt a long while after without Flame like a piece
of Charcoal or a lump or Tinder.
[Retrospective marginalia:]
5
Tbd
{circle}
h (margin, at end of paragraph)
But because I
[ 'suspected' deleted] doubted, whether every Essential Oyl as such might
be proper for this Experiment, I thought fit to make
Tryal of it with Oyl of Anise-seeds, that being different from most other
Chymical Oyls, that it will Coagulate of it self, even in moderately cold
Weather. Wherefore we took some, that
<seemd>[replacing 'was appear'd'] totally Congeal'd, (as they express it) & by that Sign
appear'd to be pure & unsophisticated; & having with Heat reduc'd it to
Fluidity, we proceeded with it as with the Oyl of Carvi; but found, that
thô the Mixture afforded Smoke, yet it afforded no Flame at all. So great
an interest has Texture in this Affair.
[Retrospective marginalia:]
6
Tbd
{circle}
h (margin, at end of paragraph)
To shew that among fluid Essential Oyls, that of Carvy is not the
single one, that is fit to afford a Flame; we took about the bigness of a
Walnut of Cotton, & having drench'd it in Chymical Oyl of Juniper, &
press'd it a little to free it from superfluous Liquor, we put to it in a
Copper Spoon,
<some>[replacing 'some'] of our strong Vitriolic Spirit of Nitre; upon which it did
immediately, as we expected, send up, together with copious Fumes, a
[BP 21, p. 221] large & vivid Flame that was very yellow, &
lasted for a while; but being then blown out; did not rekindle of it self, nor by
holding
[ 'the' deleted] it so that the Fumes reach'd to an actual fire.
Wherefore for greater security, we
[ 'repe' deleted] reiterated the Experiment
carefully, but observ'd little that was peculiar in it, save that when the
Flame broke forth of it self, it did it with a surprising Noise, equal, by our
guess, to that which half a pound, or a greater quantity, of Gunpowder kindled
in the free air, would have produc'd.
[Retrospective marginalia:]
7
{circle} (margin, beginning of first paragraph)
Tbd (margin, beginning of first paragraph)
h (margin, at end of first paragraph)
h (margin, at end of second paragraph)
To try whether Cotton were necessary to our way of producing Flame,
[ 'I' deleted] as we presum'd a Body analogous to it, thô not, as the
Chymists speak, of the Vegetable, but of the Animal Kingdom, would not be as
proper we took about the quantity of a Walnut of black Wool (not so much
because it is thought of a hotter nature, but because we had no other at hand)
& having well moisten'd it with Chymical Oyl of Carvy, we put to it some of
our Vitriolic Spirit of Nitre, & presently had (what we look'd for)
<such> a copious & blazing
[ 'yellow' deleted] Flame of a yellow Colour, that this
<Accension>[replacing 'Experiment'] seem'd to be
<somewhat> more easily produc'd than in any of the former
Experiments.
[I have several times thought, that the Accension produc'd by the
mixture of Bodies Cold as to touch, depended Mainly (for I do not say Only)
upon this; That by the Mixture of these Bodies there is produc'd such a change
of Texture, & particularly as to Pores, that either the more Spirituous
& active Ingredients are set at Liberty &
<powerfully> Excited, or the
<translucent> æther is
determin'd to excite in the Compound Body
<such> a
[ 'very' deleted] vehement & tumultuous Agitation of the minute parts,
as is sufficient to put them into that State wherein we call the Aggregate of
them Flame. This Opinion or Conjecture I thought fit
to examine by some Tryals, wherein thô the chief Agent & most active
Ingredient was still retain'd & made use of, yet
<there should be a Change of>[replacing 'the']
one[altered from 'other'] or other
<of the two remaining> Ingredients, but especially of that which
is
[ 'by most' deleted] commonly reputed by Chymists, & not by them alone,
to be the proper Seat of Inflammability, if not the only Fuel of Fire. To make
this Examen, I
[ 'pitchd upon' deleted] thought fit to substitute Wooll to Cotton, &
so to vary the Oyls I would imploy, that my choice should comprehend
Inflammable Liquors of very differing sorts, & indeed of as many of those
that then came into my thoughts, as I
[ 'then could' deleted] had then
[ 'at hand' deleted] within my power [BP 21, p. 222] And, to
comply with my present hast, I shall for brevity's sake, make use of Barbarous
but Compendious Names, & call the Experiment
formerly describ'd
<sometimes> Phlogistic, sometimes
Flammiferous, but most commonly Flammific, from the
Flame that it dos, or is at lest design'd to produce.
[ '[approximately 1 character illegible]' deleted]]
[Retrospective marginalia:]
8
Tbd
{circle}
h (margin, at end of paragraph)
We took Spirits totally
[ 'Ardent' deleted] Inflammable, such being lookt upon by Chymists, as
<a>[replacing 'the'] highly rarefy'd Sulphur (of Vegetables,) & the proper
Principle of Inflammability; & having with this, instead of an Essential
Oyl, made the Flammific Experiment, after the manner
<already>[replacing 'above'] more than once recited, we did not find that the Commixture
produc'd any store of Fumes, much less any actual Flame. And,
[ 'that' deleted] which seem'd somewhat odd, the Cotton was not burnt
to['o' at end of word deleted] any thing
near Blackness, nor so much as
[ 'made' deleted] brought to be rotten or very soft
[Retrospective marginalia:]
9
Tbd
h (margin, at end of paragraph)
Because Experiments made for another
purpose, & elsewhere
<related, make it probable that in
[ 'Alcol' deleted] Spirit of Wine, thô diligently rectify'd,
the Sulphur or Oyl of the Wine is very much attenuated; I thought fit to make a
considerable variation of the Experiment, by trying it with a Liquor that
seem'd to be very much of kin to an Essential Oyl of Wine; & yet is made of
Wine by the help of no other Ingredient than Vitriol. For this Liquor is a true
Oyl that will not mixe with Water, as the abusively call'd Oyls of Vitriol,
Tartar &c. will do. Nor is it Acid, but tasts when it is well made like
<
an>[replacing 'some peculiar kind of'] Aromatic Oyl, & is like it also in subtlety of Parts
& Penetrancy. But having moistned Cotton with this Liquor, & put our
Menstruum to it, thô there was a great Tumult excited, accompany'd with
very copious Fumes,
it[altered from 'that'] appear'd as
red as Fire, yet there was not any real Flame produc'd.>[insertion in margin ]
[Retrospective marginalia:]
10
Tbd
h (margin, at end of paragraph)
Expressd Oyls abounding in an Inflammable Ingredient, much more
Dense than that which
[ 'predomi' deleted] constitutes high rectify'd Spirit of Wine, & even
than that
[ 'which predomi' deleted] of the Essential Oyl of Carvy; we thought fit to
try with
[ 'this' deleted] this more heavy Liquor, the Flammiferous Experiment. And
having with good Oyl of Olives,
[ 'tak' deleted] (as that
[ 'most common & le' deleted] which seem'd the fittest to be made an
Instance of express'd Oyls) & proceeded in the rest of the Tryal after the
usual manner; we observ'd that upon the commixture of the Ingredients, a great
tumult
[ '& a' deleted] was excited & a pretty deal of Smoke emitted, but
no Flame at all ensued; but the Cotton was by the corrosive action of the
Menstruum
[ 'mad' deleted] brought to be very rotten or soft, & of a dark
<
[ '& alb' deleted] or somewhat blackish> Colour.
[Retrospective marginalia:]
11
Tbd (margin, at first paragraph)
h (margin, at end of first paragraph)
Tbd (margin, at second paragraph)
h (margin, at end of second paragraph)
After all the foregoing Tryals made with our Phlogistic
Menstruum upon Oyly Liquors, we thought fit to make
one upon a Substance that was not Fluid, nor easy to be mix'd with
<al>most
<any> of the Oyls we had for other purposes long ago
attempted to unite it with. We cut off then a little bit of our Glacial
Noctiluca or consistent Phosphorous, & lapping it up in a convenient quantity
of
<dry> Cotton, we put a little of our kindling Spirit upon
it, & stirr'd them a little to give the easier access to the
Menstruum. Whereupon the Mixture suddenly took fire,
<(which was> accompany'd with a pretty deal of Smoke), &
afforded us one of
<a more>[replacing 'the most'] vehement white vivid & almost dazling Flame
[BP 21, p. 223] than could well have been expected from so small a
quantity of Fuel. And after the Flame was expir'd the remaining Matter sent
forth store of Fumes, but
[ 'by far' deleted] neither so dark nor so red by far as we have
observ'd in divers of the foregoing Experiments.
And when we had for tryals sake put a little bit of a well kindled Coal upon
the soft matter that remain'd in the Spoon, this Coal was thereby kept in a
kind of dancing motion so long, that the Bystanders justly admir'd it,
especially since it was not overcast with Ashes, but kept alive as if it had
gently blown all the while.
But, because I thought it might be suspected, that the
<abovemention'd> stirring of the Ingredients to mingle them,
thô it were done very faintly might contribute to the accension of
them[altered from 'the']
[ 'agitated Mixture' deleted] by reason of the Disposition of the
Phosphorus to be kindl'd by Agitation, we did for the
greater security reiterate the Experiment without
stirring together the Ingredients as before, & yet there was produc'd a
Flame
<
[ 'so' deleted]> exceeding fierce & blazing almost to a wonder,
<accompany'd> with a pure & extraordinarily vivid Light,
& the Matter remaining in the Spoon after the exspiration of it, continu'd
for a considerable while not only to
[ 'throw out Fumes' deleted] Smoke but to boyle.
[Retrospective marginalia:]
12
Tbd
{circle}
h (margin, at end of paragraph)
The black Liquor that goes under the Name of Barbadoes Tar, because of some resemblance it has to that
vegetable substance, in point of Colour & some other Qualities & Uses,
is
<yet held to be>[replacing 'indeed'] a Mineral Liquor; &
[ 'by' deleted] a
[ 'man of' deleted] literatet
person that gather'd it in the Island of Barbadoes, assur'd me that it was a Bituminous
Substance, which He had found gliding from Rocks on the Sea-side; so that it
seems to be a coarse kind of Petroleum. Wherefore to
make our Experiment upon a true Bitumen, we took some of this Liquor, which thô
esteem'd very penetrating of it self, we had for other purposes made more pure
& subtil by Distillation. We took, I say, this Oyl of Barbadoes Tar, &
having moistned Cotton with it (in one of the Spoons hitherto often imploy'd)
we put to it our
<kindling>[replacing 'Nitrous'] Menstruum; but found less Commotion
& Smoke to be produc'd therby than we had observ'd in any of the
Experiments recited in this Paper. Only the Cotton
<was observ'd to be>[replacing 'appeard'] somewhat alter'd, especially when stirr'd with a stick of Glass,
appearing to be not of a black but of a red Colour;
[ 'yet' deleted] nor did it, [BP 21, p. 224] for
<all> that Colour, so easily take fire at a piece of lighted
Paper, as Cotton in other Tryals is wont to do.
[Retrospective marginalia:]
13
Reg of {antimony} & {copper} (in uncertain-Greg hand)
Tbd
lb.i of {antimony} & lb{half} of very good
Copper
[ 'affor' deleted] being melted together & cast into a Cone, afforded a
Regulus weighing five ounces & {drachm}
v & a solid Recrement weighing fourteen ounces &
{drachm} i (which seem'd to have a pretty deal of Reguline
Matter remaining in it) besides {drachm} xiii {half} of
Recrement that was not solid.
[Retrospective marginalia:]
14
{sulphur} of {antimony} (in uncertain-Greg hand)
Tb'd
h (margin, at end of paragraph)
lb i of {antimony} & lb.i of good Oyl of Dantsic {vitriol} being mix'd together &
distill'd ex arena by degrees of fire, afforded above
{drachm} vii of fine yellow Sulphur, that sublimd into the
neck & upper part of the Retort; & then by a Mischance (the Fire being
too much increas'd) the Receiver was blown off from it. But being rejoyn'd to
it, & the operation continu'd; we had
<near {drachm} vi {half} > more Sulphur
sublim'd, but mix'd here & there with black Antimonial matter, from which
'twas not easy to separate it fully. So that the whole amounted to above
{drachm} xiii 1/2
[space of 15 lines]
[Retrospective marginalia:]
15
Tbd
{circle}
Q
We took two bits of our Icy Noctiluca,
each being about the bigness of half a small pea, & having put them into a
Copper Spoon, without Cotton or any Consistent Body besides themselves, we put
upon them some of our Flammific Menstruum. This for a
while scarce appear'd to work upon the Phosphorus,
[ 'not' deleted] scarce producing so much as a manifest Smoke. But a while
after the Fumes began to rise: & thô the Spoon did not seem to be
considerably heated, yet there was a great Commotion
between['be' altered from 'in'] the Fluid
& Consistent Substances; whence issu'd first many Fumes, & presently
after a sudden & loud eruption of a Flame, which was very large, & was
so white & vivid that it dazled our Eyes,
[ 'And soon after th' deleted] but
<it> quickly vanish'd; & soon after it was succeeded by
another, dazling &
[ 'quick' deleted] very
short['lye' at end of word deleted]
<liv'd>[replacing 'vanishin'] Flame, that seem'd produc'd as it were by way of Explosion, by the
accension of the second
Fragment[altered from 'Arg'] of the
Noctilucal Matter.
[BP 21, p. 225]
[Retrospective marginalia:]
16
H.B. congeald. (in uncertain-Greg hand)
Tbd
h (margin, at end of paragraph)
Divers ounces of well condition'd Human Blood, having been in sharp
frosty Weather expos'd to the cold air for many hours, the whole mass seem'd to
be congeal'd throughout, & was firm enough to have portions of it differing
in shape & bigness, cut out with a knife. One of these portions that we
more particularly consider'd, seem'd to be stuff'd with
[ 'little' deleted] thin plates of Ice, variously
[ 'seemed' deleted] situated in the mass, & very numerous; & on the
outside or superficial parts, there appear'd several tufts of thin plates, that
had their edges in the surface of the lump, & had the appearance either of
the Crystals of Salarmoniac dissolv'd in Water, or of little Fans display'd.
[Retrospective marginalia:]
17
{copper} cemented with {sulphur} (in uncertain-Greg hand)
{ounce} iii of fine Copper cut small being
cemented with common Sulphur for above an hour, in a Crucible with a Cover
luted on it, were made pulverable: & thô the Sulphur appear'd to have
been burnt away, yet the mass was found {ounce} iii +
{drachm} v + 43 gr.
1689
[Retrospective marginalia:]
18
{gold} & {silver} in {water} (in uncertain-Greg hand) (margin, at first paragraph)
{cross} (margin, at first paragraph)
Hydr. Jarr in Hydr. oyl of Turp. (in uncertain-Greg hand) (margin, at second paragraph)
q (margin, at second paragraph)
A Mixture of gold & Silver weighed ten picols. A mass of Gold
& a lump of Silver (each of the same weight of ten picols) were also taken.
The mass of Silver weigh'd in Water lost half a pound of its weight in the air.
And the mass of Gold lost one
[ 'tenth' deleted] 9th of a pound.
The Hydrostatical Jar weigh'd
in the air
{drachm} vi +
51 gr.
in Oyl of turp. [ 'in Water' deleted]
{drachm} iv +
23 gr.
[Retrospective marginalia:]
19
NB Exp. with {mercury} {lead} & Tinglass (in uncertain-Greg hand)
{cross}
We took {ounce} ii of Lead & as many of
tinglass & having melted them together, before this Mixture was cold we put
to it {ounce} iiii of Mercury. Of this
<
[ 'liquid' deleted]> Amalgame we strain'd {ounce} vii + {drachm} ii through shammy Leather
& of those being committed to distillation there came over into the
Receiver {ounce} iv + {drachm} iii
& the remaining Caput mortuum amounted to {ounce} ii +
{drachm} vi.
[Integral marginalia:]
March 27
[Retrospective marginalia:]
20
Ice produc'd by {sal ammoniac} (in uncertain-Greg hand)
{cross}
About lb{half} by our guess of powder'd Salarmoniac, having a pint
or better of common Water put upon it in a glass Retort whose outside was
sprinkled & wetted with the same Liquor, the Ingredients being moderately
shaken together the Mixture grew so intensely cold, that in about a minute of
an hour according to conjecture, the external Water was turn'd into Ice that
could be & partly was scrap'd off with a Knife on whose Blade it
[ 'st' deleted] was at [BP 21, p. 226] first a consistent Body,
but then quickly melted.
[Retrospective marginalia:]
21
Crystalls of sea salt (in uncertain-Greg hand)
{cross}
lb i of Bay salt being dissolv'd in Water,
filtred, & set to Evaporate, the first Crystals taken off from the surface
of the Water & dry'd, amounted in weight to {drachm} v
{half}. The next that stuck to the bottom & sides of the vessel, & was
taken off in an entire Cake, weighed {ounce} ii +{drachm}
v.
[Retrospective marginalia:]
22
How much sp. of {urine} satiates good oil of {vitriol} (in uncertain-Greg hand)
(A Jamaica Metal that look'd like pale Copper weighed
in the Air
{drachm} v +
53
in Water
{drachm} v +
17
So that its proportion to an equal bulk of Water was as that
of 9 8/10- to 1.)
June
10
[Retrospective marginalia:]
23
Increase of weight in
{gold} fulminans
{cross}
Tbd
Two drachms of
[ 'wet' deleted] fine gold (commonly called water gold) being dissolved
in good common {aqua regia} & præcipitated with {oil} of {tartar}
p. d. though the calx were carefully
edulcorated & dryed, yet the {gold} fulminans was
<found> to
[ 'have gain' deleted] exceed about 40 gr. the weight of the {gold}
first taken.
spirit of May Butter distilld in a retort & not yet rectifyed
appeard to be
<of an> acid rather
<than>[in pencil ]an urinous nature, for it made syrop of
violetts more purplish then before it destryd[correct reading is destroyed] the blew colour in our double tincture, &
made an ebullition when pourd upon salt of tartar
[Retrospective marginalia:]
25
{urine}ousnesse of
serum of blood.
Tbd
Serum of sound humane blood though it was kept about a day & a
night after the blood was drawn did yet retain so much volatile spirit that it
<readily>[replacing 'regularly'] restord the blew colour to som of our double tincture that had
been deprivd of it.
[ '&' deleted]
[Retrospective marginalia:]
26 (margin, at first paragraph)
acidity of an essentiall {oil} (margin, at first paragraph)
{urine}ousnesse of the white of an egge (margin, at second paragraph)
2 (margin, at second paragraph)
Tbd (margin, at second paragraph)
Common water that had been thrice distilled over (in a retort) with
[space of 10 characters] part of (new
english) essentiall oyl of origanum & carefully separated from it, did both
smell & tast strongly enough of the plant, & being dropt into
<2 distinct parcells>[replacing 'our some'] of our double tincture, quickly deprived them of their blew
colour
The glare of a fresh egg
<beaten>[replacing 'was beaten'] to water did discernably but yet very faintly restore
<
some>[replacing 'the'] blewnesse to the disanimated chromatick tincture
[Retrospective marginalia:]
27
good Exp. about
fire
Tbd
To examine what proportion of combustible matter may be contained
in a body destroyed by a slow fire & without actuall flame (we took one of
(the larger size) of) those
perfums['s' altered from 'd'] that by
some are
stild['e' originally between 'l' and 'd' deleted] candele pre fumo,
& having put it into the scale of a good balance wherein it was found to
weight a dragm wanting a grain (59 gr:) we kindled it at the top & let it
burn down leisurely to the very bottom & found that the ashes remaining in
the scale amounted to four grains.
[Retrospective marginalia:]
28
a viper poyson'd
Jun. 10.
Tbd
We tooke a somewhat large & dark coloured viper & having
(by pinching her throat) forc't her to open her mouth wyde we let fall into it
first one drop & very soon after another of
<our>[replacing 'a'] tobacco poison
[ '& letting go the vip' deleted] This done we let go the viper &
observed it to be very uneasy by her restless & disorderly motions &
her body appeard to be swelld, then she quickly fell into convulsions, & at
the end of about 4 minutes &
<[approximately 1-2 characters illegible] after
she had taken the liquor> she was found to be
[ 'poi' deleted] dead
glasse of {lead} weighing in the air {ounce} {half} gr
ii did weigh in the water {drachm} iii gr xvii, so the proportion was found
to be as, 5 1/2 to 1.
Some green pease & green
<beans> were separately distilld in retorts placd
<in sand> the unrectifyd liquor of each of them appeard to
[ 's' deleted] contain some volatile or urinous salt or spirit (though but
in a very small proportion.) for it readily precipitated
<out of> the solution of sublimate a white substance; &
allso turnd syrop of violets green.
[ 'F' deleted] but these effects seemd to be better performd by the liquor
drawn from the beans, then
<by>[replacing 'from'] that afforded by the pease, both these liquors being set to
rectifie, & two spoonfull or two that first came over from each of them,
being taken off their tast was but faint, nor did they much better then
[ 'the unrectifyd liquor' deleted] unrectifyd liquors perform the
forementiond experiments. Yet they (thô but faintly) restord a blew
colour to some double tincture, that had been
[ 'rectif' deleted] depryvd of it.
Tinn ore weighed, in the air, {ounce}. i.
{drachm}. ii. g. vi. In water
{drachm} vii. {scruple} ii gr.x. so the proportion of the ore to an equall bulk of water is
as 3 69/78 to 1
The mundick sparre. Weighed in the air
<{ounce} {half} {drachm} {half} g. vii>[replacing '{ounce} ii {drachm} i g. viii'] In water
[ '{drachm} i' deleted] {drachm} iii g. xv so the proportion is as 3 31/82
to 1.
A red stone got in England weighd in the air {ounce} ii {drachm} i g. viii. In water {ounce} i {drachm}
iv {scruple}i g. vi so the proportion is as 3 142/302 to 1.
a
<peice of> native pellucid
{sulphur} brought from mount Ætna in the air weighd {ounce} {half}
{scruple} i g. ii in {water} {drachm}
ii {half} i.e. in air 262 gr. in {water} 150. so the
proportion is as 1 112/150 to 1 of water
Bismuth in air weighing
[ '{ounce} iii {drachm} vi
{half} in {water} weighd' deleted] {ounce} i {drachm}
ii {scruple}i g. xv in {water} weighd {ounce} i {drachm}
i {scruple}i g. viii3/4 therefore its weight
[ 'to' deleted] is as 9 1/3 to 1 of the same bulk of water.
[Retrospective marginalia:]
43
marcasite of {vitriol}
in {water}
Tbd
Marchasite of {vitriol} in the air weighd {ounce} iii {drachm} vi {half} in {water} {ounce}
iii gr ii therfore the proportion is
as 4 278/388 or 2/3 præter-propter to 1. of water.
[Retrospective marginalia:]
44
brothe long kept
sweet
Sept: the 7th
Pres
Tbd
Four Ounces of pretty strong Jelly
Broth
[ 'being' deleted] were put up in a viol with one ounce of Totally
Inflamable Spirits & the Orifice
[ 'being' deleted] of the Vessell being Carefully stop'd with a Cork
& that sealing wax
[ 'after' deleted] it was set aside
Aug the 29 to be kept for tryall
dureing a Twelve month at least & accordingly the Vessell
[ 'be' deleted] having been this day (viz)
Sept: the 7 of the then following
year open'd the Broth smelt sweet & well for ought we perceived as at first
[BP 21, p. 228] for which reason the glass being againe closed as
before
<is>[replacing 'was'] set aside for further Tryall.
A A sprig of mint weighing
[ 'as much as' deleted] thirteen graines was
<
July the first> put into a viol
furnished with destild water & being taken out (because it began to wither)
Sept: the 6th & dryed in a napkin was
found to weigh twenty Nine grains
At the same time (viz
[ ')' deleted]
July the first) A sprig of Sweet Marjorum
weighing thirteen graines was put into a viol furnish'd with Destild water
& being taken out at the same time
<with the former> & dry'd as before was found to weigh
twenty four graines.
[Integral marginalia:]
Oct. 1
[Retrospective marginalia:]
47
obs. about colour of
flame
{cross}
A piece of paper dipt
in a strong solution of french {verdigris}, thô as the Laborant did
(& as I think truly) affirme made but in common water did when cast upon
the fire afford a flame ting'd with a fine blew
[ '& some' deleted] but not alltogether unmixt.
[Integral marginalia:]
Oct. 6
[Retrospective marginalia:]
48
obs. about 2
Thermoscopes
The Tall Mercurial weather glass
was at No 19 this morning it being a white frost.
[Retrospective marginalia:]
49
obs. about 2 Thermoscope
The small Thermoscope was a little below No 2.
[Integral marginalia:]
oct. 18. 89 (above centre)
[Retrospective marginalia:]
50
Weight of {urine}
& harsh {water}
oct 19
{cross}
the glasse bubble in
Mr Smiths
<the stone cutters> pump water weighs {drachm}
i g. xxvii lesse by 1/4
[Retrospective marginalia:]
51
Weight of {urine}
& harsh {water}
22
The same bubble in Mr
Boyl's urine weigh'd {drachm} i g. xxiv.
[Integral marginalia:]
23
[Retrospective marginalia:]
52
a snake like
marcasite in {water}
{cross}
A marchasite shap'd like a serpent without a head weighd {ounce}
i
[ '{drachm}iv' deleted] {half} gr. iv in the Air, & in the water weighd {ounce} i {drachm} i g. vii
so its proportion is as 4 16/177 to 1 of water of the same bulk.
[Retrospective marginalia:]
sp. of {sal ammoniac}
with oyter shells
There was taken {calx} of oyster shells & pouderd {sal ammoniac}
of each three ounces, being mixd there was put to them as much water as would
wet them (guess'd to be between an ounce & an ounce & an half these
being
[ '{distill}' deleted] destilld in a retort placd in sand afforded about of
[ 'the' deleted] spirit of {sal ammoniac} moderately strong.
[Integral marginalia:]
Nov. 1
[Retrospective marginalia:]
53
our thin {mercury}
in {water}
The thin {mercury} in
[ '{air}' deleted] air weighd {ounce} i {drachm}
i g. xxiii in {water} {ounce}
i {scruple}i g. xxii so the proportion of that {mercury} to {water} of the
same bulk is as 13 30/41 to 1.
[ 'c' deleted] Common {mercury} in the air weighd {ounce} i {drachm} iii {half} g. vi 1/2 in {water} {ounce} i {drachm}
ii {half} g. xv {half} so the
proportion of
[ 'the' deleted] its weight to that of {water} is as 13 43/51 to 1.
[Integral marginalia:]
nov. 5 (above centre)
[Retrospective marginalia:]
54
A pound of {oil} of
Rosin with {lime}
Rosin being powderd & well mixt with
<a pound & an half>[replacing 'twice its weight'] of quicklyme reduc'd allso to powder & destilld in a
retort, plact in Sand afforded a copious oyle not butterlike or thick like that
of wax but transparent
<thô> of a deep colour which was a brownish red
[Retrospective marginalia:]
55
Tbd
h (margin, at end of paragraph)
To enable my self to make the better estimate of the frigefactive
power of severall salts dissolved in water, we put this evening into a somewhat
tall
<drinking> glasse, the ball of a seald & gagd
Thermoscope, the globulous part whereof was externally about
[BP 21, p. 229]
[ 'in dia' deleted]
[space of 10 characters] in diameter,
[space of 17 characters] & the stemme
or pipe was about [space of 4 characters]
inches in hight, the cylindrall cavity being
<by our guesse> about
[space of 12 characters] in diameter,
then we did somewhat more then cover this ball with water, taken out of a
glasse vessell, wherein enough had been put in for all the subsequent tryalls,
<in>[replacing '&'] this water we sufferd the Instrument to rest a pretty while,
till the Included liquor was supposd to be of the same degree of coldnesse with
the ambient, & then applying it to the frame furnishd with division, whence
we had remov'd it to manage it more conveniently we observd the tingd
{spirit of wine} to stand at a quarter of an inch & a half of an inch above the
place markt frost
Then four ounces of beaten Nitre being put in together, to be sure
the liquor should have more salt then it could dissolve, the sp. was observd
quickly to descend & presently to subside above an inch, & then fell
lower & lower till it rested an inch & a quarter below the line of
frost
<whence>[replacing '&'] after a little while it began to ascend again, so that its
whole descent amounted to
[space of 2 characters] inches, this done
we tooke out the weather glasse, & sufferd the Sp: of W. to remount which
it did speedily enough, & having emptyed & made clean the drinking
glasse, & furnished
<it> with
[ 'the same' deleted] water from the same
[ 'w' deleted] vessell whence that
<for the> Saltpeter had been taken wee put in the
thermoscope, & suffered it to stay as before, & when we judg'd it to
have stayd a competent tyme, to reduce it to the
[ 'temper' deleted] coldnesse of the water we put into it four ounces
of a pulverisd mixture consisting of two ounces of niter & as much
{sal ammoniac} this made the {spirit of wine} descend much more hastily then the
former & in no long tyme it subsyded from
[ 'i' deleted] inch & a half below the lyne markt temperate to
another lyne within an inch & a quarter of the bottome of the stem so that
it subsyded in all
[ 'black makes[?] inches' deleted]
[space of 2 characters] inches, & to
try that upon the by when the
[ 'red' deleted] colourd spirit would fall no lower we removd the
[ 'th' deleted] ball of the thermoscope into a glasse furnace with
water taken out of the first nam'd
[ 'vess' deleted] glasse cistern,
by[altered from 'in'] which liquor as
a denser ambient the spirits seemd to be impelld up more nimbly than it would
have
<been>[replacing 'done'] by the
Air['A' altered from 'a']. Thirdly
having empty'd & clean'd the glasse & furnish'd with water out of the
same cistern we put the Instrument to be refrigerated by it as much as
<that>[replacing 'we'] could do it,
<then> wee put into the glasse four ounces of meer
{sal ammoniac} without mixture, which
[ 'pre' deleted] soone made the tingd spirit
<precipitately>[replacing 'hastily'] descend,
[ '& aft but when the
<frigorifick> virtue of the salt was' deleted] from below 2
Inches beneath the lyne of temperate
[ '&' deleted] towards the bottome,
above['ve' altered from 'ut'] which
[ 'it' deleted] the
place['e' altered from 'm'] it rested
at was but an inch & a quarter. so that it fell
<
but little or>[replacing 'no lower'] but little or not all lower, then
[ 'wher' deleted] formerly when the mixture of salts made it subsyde.
Afterwards we proceeded in the same method with four ounces of bay or sea salt
but found that it made the colourd sp. subsyde much above half an inch, &
lastly we made a tryall [BP 21, p. 230] after the same manner with
water of the same cistern which was kept all the while in one place, & four
ounces of good gunpowder where
<of>[replacing 'graines'] two ounces were pulverisd & the other not, by which means
the colourd sp. was made to subsyde one inch & a half below the lyne of
temperate to 3/4 of an inch below the lyne of frost, which was within half
an inch of the lowest station it had been brough to by the saltpeter.
[Retrospective marginalia:]
56
{salt} prunellæ
made with {oil} of Turp.
Two ounces of crystalls of {nitre} being melted in a crucible there
was thrown upon it from tyme some oyl of Turpentine instead of {sulphur} by
which means
[ 'a' deleted] flames were excited & sal prunellæ was made which
we designd
[ 'this way' deleted] to prepare by the help of this oyle that the acid sp.
of {sulphur} might not as in the common way, it may be suspected to be joind
with the remaining part of the {nitre} which in our Exp. was {ounce}
i {drachm} vii g. x
<that>[replacing 'which'] would no longer flash upon the injection of the oyl so that in
operation there was a diminishing of 50 grains of the first weight of the
[ '{salt}' deleted] salt.
[Retrospective marginalia:]
57
heat produc'd by sp.
{urine} & {nitre}
q
[ 'In' deleted] The tender Thermoscope marked X was put into a cylindricall
glasse such as the shopes
style['s' at end of word deleted] a
mustard glasse & into this was pourd as much rectifyd sp. of {urine} as did
more then
cover['ver' inserted above 'lour' deleted] the globulous part of
the Thermometer which was left in the liquor for a convenient tyme that the
ting'd {spirit of wine}
might[altered from 'may'] be reducd to
the same degree of coldnesse with the ambient sp. of {urine} by which it was
brought downe to the
<enammeld>[replacing 'blank'] mark above the ball. Then we dropt into it some strong sp. of
{nitre} but warily least the ebullition might make the liquors or froth
overflow: & we observed that before the {urine}ous was satiated by
{nitre}ous, the colourd {spirit of wine} was impelld up to the
[ 'blank mark' deleted]
[space of 3 characters] mark which
was[altered from 'would'] but 4 of being
the highest of all
<those of>[replacing 'in'] the instrument
[Retrospective marginalia:]
58
Zink & {copper}
colliquated
Thre[correct reading is three] parts of {copper} being
melted meerly by the force of fire one part of Zink was thrown into it &
<upon their>[replacing 'the powder'] being mixt they were into an ingot whose surface was of a
Golden colour but the masse tho in some measure it yeilded to the hammer yet it
was brittle (
yet[altered from 'that'] scarce
enough so to make good soder) & being broken show'd a grain not so much as
yellowish.
[Retrospective marginalia:]
59
Zink destroyd by
{sal ammoniac}
Twelve dragms of {sal ammoniac} being
<well> mixd with half the weight of filings good Zink &
sublimd in a small retort there ascended a considerable proportion of the sal
armoniack in forme of flowers, the remainder
[ 'which was' deleted] (for it was not a caput mortuum) which was the thing
we lookt for, was a fusible substance which by
<the> change
<of texture> we designd to produce had quite lost all appearance
<not only> of
[ 'the pre' deleted] Zink, but of any metalline body
A litt
[Retrospective marginalia:]
60
[ 'oyl' deleted] odde [mixture] of {oil} of
{vitriol} & {oil} of aniseeds
Tbd
A little
<of> unsophisticated, & coagulated oyl of aniseeds was
put into a small wyde mouthd glasse, & some good oyl of {vitriol} dropt
upon but thô there was in a trice producd a fine & intense rednesse
in the mixture yet it did not appear that the oyl was dissolvd & brought
into a fluid state, thô to facilitate the dissolution the mixture was
[BP 21, p. 231] stirr'd to & fro with a stick of glasse.
[Integral marginalia:]
Dec. 7. 89
[Retrospective marginalia:]
61
smoaking {spirit} of
{salt} not flammifick
h (margin, at end of paragraph)
To try whether another {salt}ine Menstruum then our flammifick one if it were made exceeding
strong would not be
[ 'added' deleted] able to kindle {oil} of Carawayes we prepard some sp. of
{salt} after a peculiar manner which made it exceeding strong
<so that>[replacing '&'] when the viall 'twas kept in was at any tyme opend it would
presently emitte a thick (thô white) smoke. But this so corrosive spirit
it self being put upon cotton drencht in oyl of Caraways in a copper spoone
after our usuall manner did scarce produce any sensible
[ 'heat' deleted] warmth in the spoone & did not only not take fire but
emitted fumes themselves spareingly enough. The cheif[correct reading is chief] operation I observe being that by degrees the cotton
& other stuffe that was in the spoone grew
[ 'of' deleted]
<a> darker & darker colour, & at length became allmost
quite black, but the flame it afforded when a bitt of lighted paper was held to
it, was
<very> yellow & lucid.
[Retrospective marginalia:]
62
butter of
{nitre}
Twelve {ounce} of
[ '{nitre}' deleted] crystall of {nitre}, & as much {oil} of
<{vitriol}> being {distill}d by degrees of fire & at
lenth[correct reading is length] so strong for divers hours that the
bottom of the glasse retort melted afforded {ounce} ii of
<very>[replacing 'the'] dry
[ '{caput mortuum}' deleted] & white {caput mortuum} & which is
unusual about two dragms by guesse of a substance
[ 'in co' deleted] that lodgd it self near the mouth of the
[ '{retort}' deleted] retort was in colour & consistence very like
butter of {antimony}, 'twas
all[altered from 'allso'] very corrosive
<& ready> to
<attract or imbibe>[replacing 'undru'] the moist air.
[Retrospective marginalia:]
63
[ 'od' deleted] odde production of cold & heat
Nov. 9. 89
Tbd
To confirme what we have elsewhere deliverd about the
Mechanical origine of heat &
d cold wee devisd the following Experiment. wee tooke a small & hermetically seald
Thermoscope whose stemme was divided into parts equall enough as to sense by
little specks of amel that sharp liquors might not eat off, or spoile the
marks. The ball of this Instrument we put into a slender cylindricall vessell
(calld in the shops a mustard glasse) & more then coverd with strong
<oyl of {vitriol}>[replacing '& rectifyd sp. of Nitre'] & left
[ 'it' deleted] there a while to be reducd to the temper of the surrounding
liquor;
<Then> We cast upon it by degrees
[ 'th' deleted] grossely powdered {sal ammoniac} which presently was wrought
on
[ 'by' deleted] furiously by the Menstruum
<&> by
<this>[replacing 'which'] conflict was producd a seeming effervescence with great noise
& store of froth which more then once
[ 'requird care' deleted] was ready to run out of the vessell.
<But for all>[replacing 'Whilst'] this seeming ebullition
[ 'lasted' deleted] the mixture instead of growing hot did really grow cold
<or & colder> as appeard not only when the vessell was
touchd by the fingers on the outsyde, but by a surer mark which was the descent
of the colourd spirit of wine, how
<much>[insertion in margin ]
farther[altered from 'farher'] it would
have descended
<for the liquor was not near satiated with the {salt}> we were
hindred from discovering by an unlucky accident that broke the thermo[BP 21, p. 232]meter, & put an end to
the['e' altered from 'at']
<first> part of our Experiment, But
<this was no hindrance to> the second part, which for its
noveltye wee
[ 'cheifly' deleted] mainly design'd, for when wee pourd this actually
<& considerably> cold Mixture into
three or four tymes its weight by guesse of
[ 'as much' deleted] common water
<that was likewise actually cold> this second mixture did as I expected immediatly grow so hot that I
[ 'was not fond of keeping' deleted] did not like to keep my fingers
<for> a minute or two upon the outsyde of the glass
[Integral marginalia:]
dec. 11.
89
[Retrospective marginalia:]
64
To Try whether by the help of {lime} we could turn dry {salt} of
{urine} into a
<spirit or> liquor (which probably
<as being devoyde of
[ 'fle' deleted] flegme>
[ 'would be exceeding strong' deleted] would be exceeding strong & fit
for divers good uses) or destroy it, or do partly
[ 'the former' deleted] one & partly the other we took a (nimbly made)
mixture
<{ounce} ii
[ '{salt}' deleted]> of
[ 'good {lime} &' deleted] volatile {salt} of {urine} & as much
good {lime} & put them into a small retort to be destilld in a sand
furnace. The event was that the greatest part of the {salt} came over in forme
of a liquor & retaind its fluidity whilst it continu'd in the receiver but
when it was pourd out thence into a viall
[ 'we' deleted] it
<was> quickly coagulated
[ 'it self' deleted] into a butterlike substance
The {caput mortuum} weighd
[space of 3-4 characters] & to finde
out whether what was
<not found>[replacing 'lost'] of the salt was by the
<operation>[replacing 'action'] of the {lime} turnd into a earthy substance or retaind its
saline forme we made a lixivium of the remainder of our {caput mortuum} &
[ 'with fair' deleted] when we evaporated it we obtaind not
<at most> above two gr. by our gues of a saline substance
which
[ 'made' deleted] readily enough turnd syrop of violets green, it seemd
rather to be of a lixiviall than {urine}ous nature, by its turning thô
somewhat slowly a solution of {sublimate}te yellow.
[Integral marginalia:]
Dec 25. 89
[Retrospective marginalia:]
65
Satiated Salt of
Tartar examind.
The {salt} of {tartar} satiated with distilld vinegar, & then
warily coagulated, & afterwards dissolvd in common water being dropt into a
{tincture} of lignum nephriticum did at first very much take of the blewnesse
of it, either by its saline parts as seemd not unprobable or by diluting the
{tincture} with its aqueous or by both together, but the acidity was so faint
that even at first it did not quite take off all the blewness, & after a
while that colour seem'd manifestly
<enough> to encrease a little in the mixture.
[Integral marginalia:]
Dec 27
[Retrospective marginalia:]
66
sulphureous oyl of
wyne
Eight {ounce} of oyl of English {vitriol} being by degrees mixt with
as much totally inflammable spirit, & about so much as one days previous
digestion, committed to
[ '{distill}' deleted] destillation per Retortam & the operation being
warily & slowly made wee did by these means obtain (what most
[BP 21, p. 233] Chymists would not have Expected) about an ounce of
clear
<& true> oyl that would not mix with water but readily sink
in it, the smell was not fragrant but sulphureous & extremely pierceing.
The black {caput mortuum} was taken out & put to a smaller Retort,
whence['nce' altered from 'rein'] being
destilld with a stronger fire it yeilded
[ 'some spoonfulls quant' deleted] about {ounce} i
{half} by guesse of an acid sulphureous liquor whose smell was much stronger
than its taste, & ther remaind of very dry & black
C. M. near about half an ounce.
Jan. 1. 1689/90
[Retrospective marginalia:]
67
[ 'One graine' deleted] To show the diffusiblenesse of {tincture} that may
be even in wood not considerably compact or heavy, wee put by degrees one
graine of good lignum nephriticum first
one[altered from 'once'] {ounce} of water
& after that it infusd 2 or 3 days, so much more of the same liquor as made
it up
three[altered from '{ounce}'] {ounce}
& a dragme, so that one of wood not barke communicated a visible {tincture}
to fifteen hundred tymes its weight of water, & yet the {tincture} was
double viz. yellowish & blew, & so manifest that it seemd capable of
being visible if we should
[ 'adde' deleted] make a considerable addition to the quantity of the
liquor
[Integral marginalia:]
Jan 7
[Retrospective marginalia:]
68
The spirit of wyne in great part Inflammable that
was['s' altered from 'd'] drawn from
oyl of {vitriol} in the above-mentiond Experiment viz: the
[space of 2-3 characters] was put to an
equall weight of fresh oyle of {vitriol} & destilld againe, & afforded
[ 'at' deleted] this 2d destillation a spirit somewhat like the former
save that it was more sulphureous & sharp, & containd a smaller portion
of inflammable matter, &
[ 'from' deleted] by this 2d destillation we obtaynd an oyl heavyer
[ 'by' deleted] then the sp. but which by our estimate did not much if
at all exceed a 4th part of the quantity of that we got the first tyme.
To manifest to some virtuosi the changes that a spiritualisd {salt}
may make on a corporall one whereon it does not without fire discover any
[ 'manifes' deleted] notable operation & that also by the reaction the
volatile liquor may as well have some of its parts reducd into their pristin
corporeall form as elevate
<many>[replacing 'the']
parts['s' altered from 'icles'] of the
grosse body into the form of a spirituous liquor we made the following
experiment. We took {ounce} i {half} of crystallis'd
{nitre} &
[ 'we' deleted] having pouderd it we put upon it {ounce} iv of good sp. of sea salt these we distilld together
<in>[replacing 'out of'] a {retort}
<not>[insertion in margin ] with a
<naked> fire
[ 'not naked' deleted] but only in a sand furnace & yet wee obtained an
{aqua regia} partly consisting of {nitre}ous parts as appeard by the red fumes
that after the while were passd filld the receiver
<afterward we cut the {retort} to take out> the dry
{caput mortuum} or rather the remaining {salt} which we dissolvd in fair water
& then sufferd to evaporate very slowly by which means I had as I
[BP 21, p. 234] expected pretty store of
<small> crystalls that floted on the surface of the water &
were
<of> cubicall figure
[ 'like' deleted] emulating that of sea salt. And when these grains were
grown big & heavy enough to sink, the evaporation without fyre being
continued they were succeeded by others, either of the same shape or very near
it, that fastned themselves to the syds & lower parts of the glasse, by
looking on which one would not suspect the coagulated
<salt>[replacing 'matter'] to
<have been once {nitre}>[replacing 'participate of the nature of {nitre}']
[Retrospective marginalia:]
69
To make some tryall of the subtlety of
animal[second 'l' at end of word deleted] calces wee tooke some
hearts-horn burnt very white & having powder'd it filld with it a slender
glasse pipe open at both ends
but['b' altered from 'th'] having a
little Rag tyed over the orifice of the lower to keep the Calx from falling
out.
This['is' altered from 'e'] end of
the pipe wee put into a glasse into a
[ 'somewhat f' deleted] glasse whose bottom was flattish & coverd with
Red wyne to
<the height of > about half an inch. The
[ 'p' deleted] meashes or
[ 'the' deleted] smalls pores of the Rag giving accesse to the liquor did
in 3 or 4 houres tyme ascend into the pipe by the small interstices between the
grain of the pouder,
<to> the height (by our guesse) of about 4 inches.
[Retrospective marginalia:]
70
Some rectifyd {oil} petræ being shaken together with strong
oyle of {vitriol} did not make such an effervescence as 'tis wont to do with
{oil} {distill}d from substances belonging to the vegetable or animal
kindome[correct reading is kingdom] but yet the
[ 'oyl' deleted] {oil}late {oil} grew intensely Red so as to be allmost
opacous whilst the other {oil} grew more limpid & swame at the top of it,
the surfaces of
<both of> them
[ 'being' deleted] not at all appearing confounded.
Jan. 25
[Retrospective marginalia:]
71
Fine {gold} & fine {silver} designd for experiments were melted
in equall weight; & of the mixture, which lookt white like silver we did in
a tender ballance carefully weigh out {drachm} ii in the
Air &
[ 'for' deleted] afterwards found it to weigh in {water} {drachm}
i {half} g xxi 1/8 so that its
proportion to water was as 13 52/100 to 1.
[Integral marginalia:]
Jan 25.
[Retrospective marginalia:]
72
Upon the Inducements & for the the purposes elsewhere
[space of 9 characters] mentiond wee
tooke filings of steel & put to them instead of oyl of {vitriol} (the
usuall solvent in the preparation of
[ 'le' deleted] {vitriol}lum {iron}tis) a s. q. of
<good> sp. of sea salt & made therewith by solution,
filtration & NB, by a slow & wary evaporation
<a>[replacing 'green crystaline'] salt that shot into green crystalls like {vitriol}. This
{vitriol}late substance we dryed carefully (to avoid calcining it) & then
tooke {ounce} [space of 2 characters]
which wee put into a glasse retort & destilld in a sand furnac fit to give
a strong fire: by this means, after about
[ '[approximately 2 characters illegible]' deleted]
hours,
[ 'wee had' deleted], (during
<2 or 3 hours>[replacing 'a good part'] of which tyme the matter came over in white fumes) wee obtaind
about {ounce} [space of 2 characters]
{drachm} [space of 2 characters]
[ 'for' deleted] of a spirit acid in tast like {oil} of {vitriol} &
somewhat {sulphur}eous in sent besyds which there ascended in a
[BP 21, p. 235] dry forme three sorts of matter, whereof the
[ 'middlemost' deleted] principall was in the neck of the {retort}
& amounted to near a spoonfull of sublimate or flores, that were not only
of a deep Red but
[ 'for the most part' deleted] abounded in corpuscles pretty enough
& sparkling or glittering.
[Integral marginalia:]
Jan. 28 89/90
[Retrospective marginalia:]
73
[Thô there is fallen much rain these three days last past the
<{mercury} in the> Baroscope continued more high then could
be expected & was this morning yet higher standing at about 4/10 above 30
inches]
[Retrospective marginalia:]
74
The prysmaticall crystall amounts to 3/8 of an inch its
decrement in water is 9
[ '6' deleted]
[ 'its decrement' deleted] in yellow sp. of
[ '{nitre}' deleted] {salt} it weighs 8 gr 3/4 lesse than it did in
water, & in the green sp. of {salt} it weighs 45 gr. lesse than in the
water.
[Retrospective marginalia:]
march 26.1660.
Æolipile {ounce} viii {drachm}
iii gr. v Empty'd of Air, save only
containing in it {ounce} i {drachm} iv gr. 32. The Air being let into it increasd its weight by
xi gr. so that it weigh'd in all {ounce} viii {drachm} iii gr. 13.
The Æolipile heated red hot, & immediately plung'd under
water, suck'd as much water, as together with the Æolipile weigh'd
{ounce} xxvi {drachm} ii gr. 30. The
same Æolipile quite filled with water weigh'd {ounce} i {drachm} ii g. 30 more the weight of the
Æolipile it self was {ounce} vi {drachm}
v.
[Retrospective marginalia:]
Dec. 11.
14. (margin, at second paragraph)
A full bladder weighing {ounce} i {drachm}
i gr. 42 1/2 press'd close together wanted 14 gr. of
the same weight, the same bladder filld with water weigh'd lb. xiii v {ounce}
A bladder not very hard blowne weighing {drachm} i gr. v prick'd & empty'd wanted half
a graine of the same weight the same bladder oyl'd fill'd with water, &
weighd was found to weigh {ounce} viii {drachm}
i 1/2
The great marbles 3
<inches>[replacing 'if'] in diameter moistend with oyle sustain'd eighty four pounds.
[BP 21, p. 236]
[Retrospective marginalia:]
Aug. 18 A grain of fine {gold} at the
present rate is worth 2 pence & 4/5 of a penny (margin, at top of page, next to first line)
feb 14 89/90 (margin, at line 'Another glasse bucket was found to weigh')
found to be A
English Talk (margin, at line for 'a stone resembling Talk')
march 1 (margin, next to deleted line for 'Calx of {tin}')
the weight of
hide park water equall to it in bulk is 18 {scruple} 1/2 (margin, at line 'this amber weigh'd in {air}')
this being empty weighd in {water} xxxi
1/2 grains (margin, at line 'another round glasse phiall')
A french Louis d'or in {air} {drachm} i g.
xxxxiv in {water} {drachm} i {half}
g. 8 prop.
[ 'as 27 8/16' deleted] 17 1/3 to 1 Amethyst weighs in {air} {drachm}
iii g. ix ----- in {water} {drachm}
i {half} g. xxvii 3/4 prop as 2
68/100 to 1 An
<Emerald>[replacing 'Saphire'] weighd in {air} 35 1/8 g ----- in {water} 24 31/32 g. ---
prop as 3 45/100 to 1 Seed pearl weighd in {air}
[ '{drachm} ii {half}' deleted] {drachm}
iv ----- in {water} {drachm} ii
{half} 1/2 --- prop as 2 68/100 to 1 A Spanish piaster in {air}
{drachm} i {half} g. xv 3/8
----- in {water} {drachm} i {half} g. ix 3/8 --- prop as 17 97/100 to 1. French Chalk in
{air} {drachm} iiii g. iii ----- in
{water} {drachm} ii {half} 1/4 --- prop as 2 61/100
pr. to 1 French Chalk in {air} {drachm} iiii {half}
g. xi ----- in {oil} Turp. {drachm} iii g. x 1/4 --- prop. as 3 99/100
to 1 Another glasse bucket was found to weigh {drachm} vi {half} g. 20 1/4 in {water} {drachm} iv gr. 12 1/2 Copper
Ore[originally 'oare'] of a
blew[originally 'blewer'] Colour weighd
in {air} {drachm} iii g. 1/2 ----- in {water}
{drachm} ii gr. vii prop as 3 4/10 to
1 prox Spanish {mercury} weighd in {air} 480 gr. in {water} gr. 446 prop
as 14 11/100 to 1 Benjamin of the purest sort in {air} ----- {drachm}
vii g. 17 1/2 --- in {water} {drachm} i g. xxiv prop Ivory ----- in {air}
{ounce} i {drachm} i {half} g.
xxvii 1/2 in {water} {drachm} iv g xxiv prop as 1 79/100 The long
crystall in
{oil}[originally '{air}'] of {vitriol}
{drachm} i g. xvii 1/2 ----- in
{water} {drachm} ii g. xl A
peice of red amber in {air} {drachm} v g. vi in ----- {water} g. xii prop as 1
4/100 to 1 The gl. ball weighd in Mr Boyls
{urine} ----- {drachm} i g. 23
3/4 The crystall in the same {urine} ---------- {drachm}
ii g. 38 Unicorns horne in
{air} {drachm} iv g. x 1/2
----- in {water} {drachm} ii prop as 2 8/100 to 1 a
stone resembling Talk in {air} {ounce} i {drachm}
i g. iv ----- in {water} {drachm}
v {half} g. xxxii prop as 3 1/181 to
1 the Crystall
<of 256 grains> in Strong Solution of Mercury in {aqua fortis}
Weighd {drachm} i g. v 1/4 prop:
as 1 70/100 to 1 Cornish bismuth in {air} {drachm} iii {half} g. iii 1/4 in {water}
{drachm} ii {half} g. 41 1/4 prop as 10 13/100 to
1 the crystall in {distilled vinegar} fortiori weighd {drachm} ii g. 39 in comon brandie {drachm} ii g.
45 1/4 In green sp.
of[originally '{vitriol}'] Salt {drachm}
i {half} g. xxv 1/4 in another
sp.
<of {salt}> {drachm} ii {half} g. 1
1/4. In deptford liquor {drachm} ii g. 18
bismuth ore in {air} {ounce} {drachm} i ii g. 1/2 in {water} {drachm} vii
{half} g. 48 1/2 prop as 5 94/100 to 1
[ 'Calx of {tin} in {air} {drachm} ii {half} g. 2
1/4 in {water} {drachm} ii g. 13 prop as 7 4/100 to
1' deleted] Amber weighd in Mr Boyls {urine} grains 4. in Sm. g. 11 1/2
in St C. g. iii
Talk
English in {air} {drachm} iii g. ii
1/4 in {water} {drachm} i {half} g. xii 1/4 prop: as 2 28/100 to 1 Copper ore white
{ounce} {drachm} i i g. 1 1/2 in
{water} {drachm} vii {half} g. xvii
1/2 prop. as 6 44/100 to 1 {sulphur} vive weigh'd in {air} {ounce}
i {drachm} i; g. xvi 1/4 in {water} {drachm} v g.
ii prop: as 2 18/100 to 1
<the piece of>[insertion in margin ] red amber
[siglum] in claret 8
grains 1/2 in sack 1/2 gr. in water 6 gr. 3/4 the long
crystall in sol. {sal gem} {drachm} ii {scruple} i in sol. {sal ammoniac} {drachm} ii g.
xxxiv 1/4
<in {distill} water 6 gr. 2/4> Eagle stone
<long four squard &> hollow within in {air} {ounce} {drachm}
i iii in {water} {drachm}
vi g. xxvii Cinnabar of
{antimony} in {air} {drachm} iii g. 16 in {water} {drachm} ii {half} g.
xviii prop as 7 to 1 An egge in {air} {ounce}
ii {drachm} i g. xvi in {water} {drachm} i g.
ix Turkish {gold} in {air} grains 170 --- in {water}
162 prop. as 19 13/100 to 1 Tincal in ----- {air} gr: 46 ---- in {water}
19 prop as 1 70/100 to 1 the white glasse which is finely cut with a
stopple of glasse & {silver} chain {ounce} i {drachm}
iii {half} g. x black marble in
{air} {ounce} ii {drachm} i g.
xxvii 1/2 in {water} {ounce} i
{drachm} iii prop. as 2 73/100 to 1
[siglum] another round
glasse phiall {ounce} i {drachm} iii
{half} gr. xix in {water} {drachm} vii g. xi full of
<a strong> solution of calcinaturm {ounce} i {drachm} i gr. ix
so the weight of calcinatum above water of the same bulk is 118 gr. this full
of calcinatum {ounce} ii {half} g. xxv so the weight of the liquor in air is {ounce}
i {drachm} {half} g. vi prop
[ 'as' deleted] to water of the same bulk as 1 29/100 or 3/10 prox.
the small piece of red amber in Mr Boyle {urine} gr. iv
the round glasse viall, & stopple full of milk in {air} {ounce}
ii {drachm} ii {half} g.
xxviii in {water} {drachm} vii g.
xxiv
[BP 21, p. 237]
[Integral marginalia:]
March 17 1689/90
[Retrospective marginalia:]
75
Four ounces of our Menstruum for Sulphur had almost as much of
finely pouderd Antimony put little by little into it, & the Sulphur that
emerged, being taken of with a wooden spoone, for one of metall were there
improper that which was skimmd off being dry'd amounted to between {drachm}
iii {half} &
[ 'grains iv.' deleted] {drachm} iiii.
[Retrospective marginalia:]
76
[ 'One' deleted] An ounce of high rectifyd spirits did in the cold readily
enough dissolve two dragms of {salt} of {tartar} in a somewhat soft consistence
prepared by abstraction
[ 'from' deleted] of our anomalous spirit from This solution was but a
little yellowish, was milde & adiaphorous enough in taste it would not
destroy the blew colour of the party colourd {tincture}
<&>[replacing '&'] it did
<not very>[replacing 'not very'] readily, thô it did after a while precipitate solution of
Sublimate into
[ 'a yellow s' deleted] pale orange substance.
[Integral marginalia:]
March 27. 90.
[Retrospective marginalia:]
77
About nine of the clock yesternight we did for more purposes than
one put into a strong crucible (which happen'd to be much larger than was
needfull) three ounces of fresh Quicklime, well mix'd with half the weight of
{sal ammoniac},
[ 'that' deleted] the pot was kept in a smiths forge, between a quarter
& half an houre, that the mixture tho very stubborne might be brought to
fusion, which it was but not so strong a one as that it could be pour'd out.
The
<vessell>[replacing 'pot'] being remov'd from the fire & brought home, & sufferd to
stand a while
<at some distance from>[replacing 'nere'] a fire,
[ 'that it might not which kept it from cooling overhastily' deleted], for
a certaine reason, & after it had been kept there a while the bottome of it
was put in a bason of cold water to hasten the refrigeration. This done the
lower
[ 'of' deleted] part of the melting pot was knockt of with a hammer &
the mixture which was found as we expected to be very hard, was
<with the closely adhereing fragments of the pot>
[ 'carried' deleted] carried, before it was quite cold, into a
darken'd['ken'd' inserted above 'k'd' deleted] corner of the roome,
the better to discerne, any light that might be producd, then of the fragments
strucke against a piece of [BP 21, p. 238] steel, by which it did
afford tho not readily some sparks & the person in whose hands it was,
looking very heedfully at it, perceiv'd after the percussion was over some
<small>[replacing 'shining'] luminous parts, that glimmerd like the scales of fishes, the light
I could easily perceive, but it seem'd somewhat doubtfull in the dark what it
proceeded from, till by putting ones finger upon the luminous part &
bringing it where the candle shone it was found to proceed from the mixture it
self not the vessell. Wee afterwards made severall tryalls most of them with
good effect to produce the like phænomenon, but those which succeded
best, were such as I causd to be try'd by rubbing briskly with the fragments
one against another, for by this means the light appear'd much more vivide
& much more extended.
what
[quantity] of sp. {nitre} dissolves & kept
dissolv'd {mercury} & {silver}
Spiritus {nitre}tri prepared our way
<{ounce} i {half}> dissolvd & kept
dissolvd
[ 'd' deleted] {drachm} xi of {mercury} our sp.
{nitre}
[ 'd' deleted] {ounce} i dissolv'd of fine {silver}
{drachm} v 1/2
[Retrospective marginalia:]
80
Jun. 10. 90.
The Cylindricall Syphon furnishd with {mercury} {drachm}
ii of {oil} of {vitriol} reachd above the {mercury} to 4
Inches & 5/8 of an Inch, & the like of sp. of Wyn that would
totally burn away reachd in the other leg to 9 inches & 7/8 of an
Inch.
Gur of {lead} in {air} [ '&' deleted] 844 1/2 in {water} 639 7/8 prop. as 4 12/100 to 1.
[BP 21, p. 239]
[Retrospective marginalia:]
Ap. 23. 90 (margin, next to line 'the 1/224600 of the whole weight')
Apr. 29. 90 (margin, at line 'this amber weigh'd in {air}')
May 3. 90 (margin, at line 'A piece of Red corall')
May. 1. 90 (margin, at line 'the glasse viall & stopple empty')
May. 24. 90 (margin, at deleted line '{silver} cuppled in {air}')
{spirit of wine} in the glasse viall & stopple weighd
[ '{drachm} vi g' deleted] in {water} {drachm}
vi g. xi 1/2.
[ 'or[?]' deleted] {oil} of {vitriol} in the same
<viall> weighd {drachm} xii {half} g.
xvii in water The viall full of serum of mans weighd
in {water} {drachm} vii g. xxiv. the
same in {air} weighd {ounce} ii {drachm} ii g. xxviii The
<very> small but strong loadstone weigh grains 52 1/4
The piece of amber
[siglum] in {spirit of wine}
rectif. weighs 34 gr 1/8 in common brandie it weighd - - - - - gr: 17
1/8 In English Brandie the Amber weighd gr. 16 in Sp. ardente
baccarum Sambuci 16 grains The purely white viall with a stopple of the
same & flat bottome weigh'd in {air} {ounce} i
{drachm} i g. xi 1/2 in {water}
{drachm} vi g. ix 1/2 The
metall got from the suppos'd minerall of {vitriol} {lead} & {vitriol}
{antimony} weighd - in {air} {ounce} i {drachm}
ii {half} g. xxiv in {water} {ounce}
i {drachm} i {half} g.
xxiv 1/2 prop as 10 99/100 to 1. The brasse
Cube, weighd {ounce} i {drachm} iii
g. iii 1/8. full of {oil} of Turpentine it weighd
{ounce} i {drachm} vi {half} g.
xv 1/4. so the
[ '{oil}' deleted] cubicall inch of oyl weighs {drachm} iii {half} g. xi 1/8 Argol
white & fine in {air} {drachm} iii {half} in - {water}
{drachm} i g. xvii The wax
ball weighd 210 gr. in {air} the {tin} in {air} weigh'd 230 gr both together in
{water} weighd 186 1/2 the Tin alone weighd in {water} 196 1/2
{lead} in {air} weighd 230 the wax 210, both together
<in {water}> 196;
[ 'o' deleted] lead alone in {water} weighd
207['7' altered from '6'] 1/2.
In {spirit of wine} Angl. rectific. 1 the Amber
[siglum] weighd grains 38
1/2. in another 2 drawn from the same wyne 37 graines In {water}
{lime} indifferent strong - grains 7. The amber
[siglum] in sea water long
kept weigh'd gr: 1 1/8 The oaken inch coated with bees wax weighd
{drachm} iii {half} g. x. the lead
of {ounce} {half} in the {air} & the coated cube together in water {drachm}
ii {half} g. vii 1/2 the cube
before coting weighd {drachm} iii g. xiii 1/2 the lead alone in {water} 210. the walnut
{drachm} ii g. xiii coated it weighd
{drachm} iii g. xi 1/2
the 1/224600 of the whole weight of a floating piece of wax
[ 'mad' deleted] weighing {ounce} iv {drachm}
v g. xxvi made it loose its
Equilibrium & sunk in
<the> water whereof deducting 24600 there remains 200000.
Crabs Eyes in {air} {drachm} ii {half} g. xii 1/2 - in {water} {drachm} i g.
xxiii 1/2 prop: as 2 1/10 to 1 the amber
[siglum] in phlegme of
brandy weighs 12 gr in hide park water 7 3/4. In Mr Boyle's {urine} grains
3 1/2 A piece of Red corall {drachm} ii g.
ix 1/4 in {water} g. 80 1/4 prop: as 2 62/100 to
1
<An>[insertion in margin ] Egge before rosting (in which the shell
burst toward the end) {ounce} i {drachm} iii {half} g. xv lost in rosting g.
xiii. Another before boyling {ounce} i {half} {drachm} i g. x 1/2 lost v gr: in boyling it coold
in the water the shell not breaking. the glasse viall & stopple empty
weigh'd in Sir Edmund
Kings
<purging> water 26 1/4 gr. Tutty in air weighd
{drachm} iii {half} in water - {drachm} ii {half} g. xii 1/4 prop
<as> 4 30/100 to 1 The amber
[siglum] in rectif. sp. of
milk evaporated vii 5/8 g. The Gold kept long in
digestion in {air} {drachm} iii g. xi 1/16 in {water} {drachm} iii 9/16 prop
18 19/100 to 1 a Guiney in {air} - {drachm} ii g.
ix 1/16 in {water} - {drachm} ii g.
ii 1/16 prop. as 18 43/100 to 1 Cupelld {silver} made
brittle & oddely prepared weighd in {air} {drachm} i
{half} g. xi 1/2 in
{water}[altered from '{air}'] {drachm}
i g. xxvii 1/2 prop 7 1/4
to 1
[ 'Aff' deleted] African {gold} in {air} {drachm} ii
g. L 2/8
[ 'g' deleted] in {water} {drachm} ii {half} g.
xii 1/2 prop 20 4/10 to 1 The crystall ball in
mother of deptford water weighd {ounce} i g:
L -1/4
[ '{silver} cupelld in {air} {ounce} i g.
xxii {drachm} vii {half} g.
vii -5/8 prop. as 11 24/100 to 1' deleted]
<supposd to be>[insertion in margin ] {gold} depravd by the Anti
<elixir> in {air} {scruple} iv g. 1/8
in {water} {drachm} i g. xv 1/8
prop as 16 2/100
[BP 21, p. 240]
[Retrospective marginalia:]
81[altered from '77']
May 20.90.
To make some estimate what porportion of acid salt the {salt}ine
portion of the sp. of Humane blood may be able to
mortifie, wee took {drachm} {half} of dry & hard vol. {salt} of humane blood & dropt into it
[ 'as much' deleted] strong sp. of {salt}
[ 'as suffic'd' deleted] till the conflict between them ceast & then
weighing the mixture we found that
[ 'the' deleted] quantity of
<acid> sp. of {salt}, had been
imployd to satiate the half dragm of vol. salt of
blood.
NB. 1st. That thô by the multitude of bubbles, & the noise
that accompany'd them would have made one think that the effervescence was very
great, yet there was
really[altered from 'relly'] producd as
far as I could judge by the touch no more than
<a> luke-warmness.
2. [space of 4 lines]
[Retrospective marginalia:]
[ '7' deleted]82
{spirit} {salt}
glasse
{ounce} i
{half}
g. 23
{salt} blood
{drachm}
{half}
{ounce} i
{half}
gr. LIII.
glasse {salt} & {spirit}
{ounce} i {drachm}
[7][unclear]
gr. 4.
293
424
131
{spirit} {nitre}
glas.
{ounce} ii -
ii
{salt} blood
{drachm}
{half}
{ounce} ii
{half}
g. 9
Glasse {salt} & {spirit}
{ounce} ii {drachm}
ii
gr. 5
19
125
100
[Integral marginalia:]
July 9 (90)
[Retrospective marginalia:]
[ '7' deleted]83
{nitre} not kindled by
sea salt, but by {sal ammoniac}
dry'd sea salt being cast upon an ounce of {nitre} in fusion was
violently enough decrepitated, did not produce any flame or flashes (except
perhaps once that some grains of injected {salt} seem'd to produce a little)
but when afterwards some small bits of {sal ammoniac} were cast after one
<after> another upon the same melted {nitre}, there were
producd such a tumult & such flashes as are usually observ'd by making of
fixt {nitre} with bits of Charcoale not to say such phænomena as
<may be>[replacing 'are']
observd['d' altered from 'able'] in
making of sal prunellæ with {sulphur}.
[Integral marginalia:]
July 10.
[Retrospective marginalia:]
84
[ 'The' deleted] A mixture of two parts of {nitre}
& one of {sal ammoniac} both reducd to powder was cast in by lesse than half
a spoonfull at a tyme into a glowing crucible, & did as I expected, from
tyme to tyme
fulminate['d' at end of word deleted]
& afford flashes but
[ 'not so much' deleted] inferiour to those that are wont to appear in the
making of {salt} prunellæ.
[Integral marginalia:]
July 9
[Retrospective marginalia:]
85
We melted in a crucible an ounce of good {nitre}, & then cast
on it at
<severall tyms>[insertion in margin ] some dry
vol. {salt} of {sal ammoniac} sometimes in little
lumps, sometimes in the forme of powder. But thô these prejections made a
Tumultuous agitation, yet the mixture did not at all
fulminate, nor afford any flashes, or light, notwithstanding that the fusion of
the {nitre} was so good, that the crucible was red
hot['t' altered from 'd'].
[BP 21, p. 241]
[Integral marginalia:]
Jun 5. 86.
[Retrospective marginalia:]
86
Some May butter being {distill}d in {sand} afforded a
sp. that without rectification was
[ 'of a' deleted] very penetrating both in smell & taste, its colour
was not red nor reddish, but of a somewhat dark yellow
<in> its composition acidity did manifestly prevaild for it
readily destroyd the blew
[ 'o' deleted] colour of the double {tincture} it presently began to work
upon crude corall it did not turn syrop of violets green it {precipitate}tated
a lixivium of {sulphur} & increasd its stinking smell & upon salt of
Tart. it Immediately made an ebullition
[Retrospective marginalia:]
87
The {oil} was strong & rankly sented & abounded in suttle
parts without rectif: it was readily dissoluble in totally ardent
sp.
[Retrospective marginalia:]
88
Last night I viewd a bladder, (whether a pigs or a lambs I know
not) which when lank was ty'd very strongly ab
<out> the neck & was
[ 'the' deleted] (
<by> means that need not here be describ'd) got down into the
globulous part of a pretty large bolt glasse which was afterwards
[ 'by the' deleted] carefully exhausted by the help of our pneumaticall
engine, after which the stemme of the glasse was hermetically closd, & to
secure the slender part of it was coverd with a pretty long pipe of Tin, that
was cemented on to the stem of the glass that there was not much Air in this
bladder, when it was conveyd into the bolt glasse was evident because it
<could be>[replacing 'was'] made to passe quite through a pipe that was not short into the
expanded part of the vessell & yet, while I saw it, it had
<been> by the withdrawing of the Ambient Air Allowd
[ 'to' deleted] swell to its full dimensions & yet when I saw it &
heedfully viewd I judgd it to have continud
[ 'in that' deleted] in that state ever since it first blew it self up,
& two things are very remarkable in the Experiment, one that the bladder
did not at all appear to be mouldy or putrify'd, & the other that Air
highly rarifyd or Expanded should retaine its springinesse for ought
[ 'that' deleted] appeard undiminishd for so very long a tyme for
a carefull
& sincere domestick of mine that had
[ 'formerly put me in minde of it' deleted] assisted at such experiments,
& had formerly put me in minde of this,
[ '&' deleted] asurd me that he had kept it in his custody, & for
the most part lockt it
[ 'q' deleted] up for the space of twentie year.
[Retrospective marginalia:]
89
July 19 90
four ounces of Guaiacum being burnt in an earthen pipkin afforded
but
[ '[approximately 1 character illegible]' deleted]
xxvii gr. of Ashes, the most part of which were very
white.
[Retrospective marginalia:]
90 (margin, at first line of entry)
91 (margin, against 'Liquor and the pouder' at top of p. 243)
Wee took two ounces of fl. of
{sulphur} & {ounce} i of {salt of tartar} & having
melted the former in an earthen vessell the salt was strowd upon it &
stirrd into it
<that they might>[replacing 'till it was'] well encorporate, the masse being very red,
<was taken out> & part of it being beaten in a warm
morter & alcool of wyne immediately pourd upon it before the Air had made
it relent a high {tincture} was presently extracted, upon the shaking together
the [BP 21, p. 243] Liquor & the powder upon another parcell of
the same red masse pulveris'd was pourd some rectify'd sp. of {urine} that was strong enough to have {salt}
lying at the bottome, this mixture at first appeard
opacous & very green, but after some hours the liquor
[ 'was' deleted] grew clear enough, & appeard of a good yellow,
smelling & tasting of {sulphur}. But at the bottome there lay a pretty
quantity of powder that was
<as> green as the mixture at first
appear'd['pea' between 'ap' and 'pear'd' deleted].
[BP 21, p. 242]
[Retrospective marginalia:]
Jun. 11 (margin, at line for 'Glasse of {lead}')
July 9 (margin, at line about 'The spoild {gold}')
July 22 (margin, at unfinished line for '{gold} extracted from')
Aug. 6 (margin, at fifth line, where there is a space in place of the substance measured)
March 4. 90/1 (margin, at line for 'Seacoal')
Sep. 21. 91 (margin, at line for 'My Lord Burlingtons ore')
Glasse of {lead} per se in {air} --- {drachm} ii g. LVI 1/2 in {water} ----
{drachm} ii g. 33 7/8 prop. 7 41/100 to 1 The
spoild {gold} in {air} --- 80g. in water ---- 75 1/8 prop. as 16 41/100 to
1 {gold} extracted from -----
[space of remainder of line] English
{tin} in {air} ---- XLVI 9/16 in {water} ----
XLIII 5/8 prop as 15 85/100 to 1 [space of 7 characters]
[ 'in {air} --- {ounce} i g. xxiii + 7/8 in {water} ---- {drachm} vii {half} g. iii 1/2 prop.' deleted]
Seacoal in {air} ---- {ounce} i {drachm} vii {half} g xxi ---- in {water} ----
{drachm} iii g. xviii 1/2 prop
as 1 25/100 Brittle {silver} in {air} ---- {drachm} ii g. 17 1/4 in {water} ----
{drachm} i gr LVIII 1/2 pro: 4
64/100 to 1 Tutenague in {air} ---- {drachm} ii g.
XLIX 1/2 in {water} ---- {drachm} ii gr 34. prop 10 93/100 to 1 French Guiney ---- {drachm}
i gr. XLIV 1/8 in {water} ----
{drachm} i gr 38 3/4 prop 19 37/100 to 1
{silver} 3 {gold} 1 mixture in {air} --- {drachm}
v g. 39 7/8 in {water} ---- {drachm} v g. ix prop: 11 2/247
to[originally 'of'] 1 {silver} 2
{gold} 1 mixture in {air} --- {drachm} v gr LVIII 7/8 in {water} ----
{drachm} v gr. xxviii pro. 11
62/100 {silver} & {copper} {ana} in {air} --- {drachm} iii gr. xx 1/2 in {water} ----
{drachm} iii prop 9 78/100 to 1 Lap. Amianthus in
{air} --- {drachm} ii gr. LI
3/4 in {water} ---- {drachm} i gr LVII 1/8 prop 2 2/100 Cornish bismuth ore {drachm}
v gr. 29 in {water} ---- {drachm}
iv gr. xxxv 6 4/10 to 1 White
Mundick from Cornewall ---- in {air} --- {ounce} i gr
xiv 7/8 in {water} ---- {drachm} vi gr iii 7/8 prop. 3 77/100
[ 'Supposd yellow mundick {drachm} ix {half}
gr.' deleted] Bononia Stone {ounce} i {drachm}
vii g. XLII ---- {drachm}
xi g. vii 1/8 pr. 4 33/100 to
1 My Lord Burlingtons ore ---------- in {air} ---
weighd {drachm} vii g. 19 1/2 in {water} ----
{drachm} vi g. xviii pr. 7 14/100 to
1 fyrestone in
[ '{water}' deleted] {air} --- {ounce} {half} g. xvi 1/2 in {water} ---- {drachm} ii
{half} g. viii pr. 2 6/10 to 1
[BP 21, p. 243]
[Retrospective marginalia:]
92
Jul. 24 (90)
This day there was put together into a single violl two ounces of
the {oil} of {vitriol}, & as much distill'd {water} upon whose
mixture there ensud an intense heat insomuch that the
upper part of the glasse at a good distance from the Liquors grew so hot that
the person who was employd about making the Experiment complaind that he could not well hold his
fingers there;
[ '{vitriol}' deleted] And the same day two other {ounce} of the {oil} of
{vitriol} being put to six {ounce} of destilld water the mixture
[space of 4 characters] intensly hot, but
yet was not judgd quite so hot as the
[ 'that' deleted] other. These two viols being slightly stopt were set
asyde to be digested for some tyme
July 25. 90
[ 'July 26. 90' deleted]
[Retrospective marginalia:]
93
Ten drops of Our {tincture} thô long kept, & thereby
impaired suffic'd
<so> to impregnate about if not full two ounces of destill'd
{water} that a little powder of Galls being cast into a portion of it presently
produc'd a purple colour, as deep thô not alltogether as lively as it
would have done if the Liquor had been
[ 'br' deleted] a minerall water brought from the Spaw, or Tunbridge.
Into an ounce of good Spirit of {salt} was dropt
<rectify'd> {spirit} of {urine}, (so strong that some
vol. {salt} lay undissolv'd in the bottome of it)
till the acid liq. was fully satiated with the {urine}ous {salt} of which it
was found by weight that
[space of 2 characters] had been employ'd
to mortifye the {spirit} of {salt}.
[Retrospective marginalia:]
94
Into half an ounce of good sp. of
{nitre} wee put at severall tymes as much finely powder'd calculus Humanus of a
whitish gray colour & taken out of the bladder, as it would dissolve, which
provd to amount to 33 [BP 21, p. 244] grains. When the first &
greatest parcell which was a scruple was put into the menstruum, there was after a little while producd a brisk
effervescence which made the mixture and bubbles swell
to the upper part of the glasse There were some light fæces but
inconsiderable that remaind undissolv'd
in[altered from 'by'] the
sp. of {nitre}, whose colour was not very much
alter'd by this operation.
[Retrospective marginalia:]
95
July 25 90
Good {gold} fulm. being mixt
with 4 tymes its weight of Gunpowder finely powder'd, & layd along upon a
smoot[correct reading is smooth] brick like a narrow traine of
Gunpowder was fird with a piece of well kindled coale, but thô the
[ 'black' deleted] gunpowder took fire yet the golden-powder did not goe of
with it, but made brisk cracks
[ 'b' deleted] grain by grain as the kindled coale came to touch sometimes
one graine & sometimes another. And thô to set on fire the remaining
granuls of the {gold}den powder we
[ 'qtum' deleted] lengthend the former tryal by the Addition of another
consisting of meer powder, this additionall traine blew up without making the
metalline granuls fulminate.
[Retrospective marginalia:]
96
July. 30.
One part of our factitious {sal ammoniac} made of
<the two spirits>[replacing 'spirit'] of {urine} & of sea {salt} being put to four parts of good
sp. of {nitre} made a brisk {aqua regia}. Where in
<two>[replacing 'some'] pieces of leaf {gold} being successively put, were in the
<cold>[insertion in margin ] dissolvd allmost in a trice.
To satiate two ounces of sp. of {salt}
there
was[altered from 'were'] requird
[ 'a little' deleted] a light weight a little over or under of {oil} of
{tartar}
[ 'p' deleted] p. d. of two ounces.
[Retrospective marginalia:]
97
Aug. 5. 1690
Six ounces of good sp. {nitre} being
drawn off from an ounce & a half of {sal ammoniac}, there remain'd not very
much of the {salt} at the bottom of the retort. Then new {sal ammoniac} being
added to the quantity of {ounce} i {half} the menstruum
was powr'd back upon it and drawn off with a stronger fire than before which so
encreasd the liquor that there remain'd
<in a dry form> but 100 grains that ascended into the neck
of the retort like white flores & 12 grains of
spungy black stuff that lay in the bottom of the Retort like a
{caput mortuum}.
[Retrospective marginalia:]
98
Aug. 13 (90)
We melted an ounce of good Tin, & then put to it as much
{mercury} mixing the Ingredients that they might the better incorporate; The
{amalgam} lookt prettily within that was consistent, & continued in the
figure, given it by the vessell it was made in. Being broken it lookt very
prettily, & was found very friable, as we designd it should be, To the end
it might be capable of being reducd to powder & mixt with other pulverisd
bodies fit for our turn.
[Retrospective marginalia:]
99
Aug. 14. 90
Two grains of Icy Noctiluca was put into a glasse weighing {drachm}
iv {half} cover'd with a paper full of holes.
[BP 21, p. 245]
[Retrospective marginalia:]
100
Aug.15
Having distill'd six ounces of lapis calaminaris & as much
{sal ammoniac} with a strong fire, & set asyde the sp. which was exceeding fiery, we afterwards broke the
Retort, & upon the grossely pulveris'd {caput mortuum} we put water enough
to cover it & sweeme a little above it. This
[ 'd' deleted] mixture did as we expected quickly begun to grow warm
[ 'till' deleted] & soon after
[ 'so' deleted] grew so hot that I was afraid to touch the glasse that
containd it with my hand, this heat as far as I could gueese did for sometime
<increase>[replacing 'grow more intense'], & continu'd thô not so intense yet considerable for a
pretty while after, thô when the water was first put on, the
{caput mortuum} had had tyme to be throughly refrigerated the affusion not
having been made till the third after the destillation.
The XVIII Century
[Integral marginalia:]
Aug. 16
[Retrospective marginalia:]
[ '10' deleted]1
{silver} refin'd a new
way
[ 'W' deleted] We tooke some sterling silver coynd amounting to {ounce}
i g. xii & having refind it
<our way> without cupelling or the help of {lead}
[ 'we h found to h' deleted] it appear'd to have lost {drachm}
i grains 29 & the silver that lookt fine being weighd
in water was found to be to that liquor as 10 18/100 to 1.
[Integral marginalia:]
Aug. 18. 90
[Retrospective marginalia:]
[ '10' deleted]2
ascent of wyne in
wood
As one way to discover
<in some sort> the measure the filtratration of
[ 'liqu' deleted] liquors through vegetable bodies we made choice
[ 'of' deleted] among shavings of dale boards
<of> one that was about an inch broad & pretty uniforme this
we
<gently stretch'd>[replacing 'fastn'd at both ends'] & fastn'd to a piece of wood
[ 'ty' deleted] tying it at both ends to prevent curling & to keep it
streight, this done wee put the lower end both of the frame & of the
shaving into a glasse furnish'd with a fit quantity of
<Red> wyne
[ 'which we colour we chose' deleted] as that liquor whose ascent
<by> its colour would
<
by>[replacing 'the'] best be discern'd, then placeing this instrument in an erected
posture, & a quiet place we left it there for some
[ 'place' deleted] days, & having observ'd
<that>[replacing 'it'] for two or three of these
<it>[replacing 'it'] did no more ascend we measured the tinged part of the shaving,
& found that from the surface of the stagnant wyne
<to> the upper part,
[ '&' deleted] of the
<discolour'd> shaving the distance was about 9 metres &
1/2.
[Integral marginalia:]
Aug. 23
1690
[Retrospective marginalia:]
3
Quick fixation of
{nitre}
There was taken a lb. (or 16 oz.) of crystalls of {nitre}, &
<these> being in a metalline mortar
<layd together in a heape of>[replacing 'heapt up in'] convenient shape the heape was kindled at the top, & then
the matter being successively & dextrously stirr'd (according to our way)
the parts of the {nitre} it self kindled one another, & in not many
minutes, were by this means reduc'd to a masse or lump that tasted alcalisate
enough, & was without and within to of a blew colour allmost like a
turcoise, & yet
[ 'th' deleted] of this [BP 21, p. 246] matter, the single
pound of {nitre} afforded us about xiii {ounce}
x gr. of phosphorous was set to run
p. d.
[ 'in' deleted] the
2 of Sept. the oblong crystall in
Mr Mattons vinegar weighd
{drachm} ii g. xxxvi 1/2
[Integral marginalia:]
Sept. the 12
[Retrospective marginalia:]
4
Strange attraction made
by the Noctiluca
The Ten graines of
<solid> Phosphorus that was exposed to the Aire the
2d of this month, appearing this day
wasted to the bigness of Less then a pins head the Liquor into which it was
resolved in a small clear Cake Glass
<being
[ 'not' deleted] weighed it> amounted to above forty four
graines if not (considering what
<Liquor> stuck to the
<inside> vessell) full 45 graines, that is about 4 times
& 1/2 as much as the Noctiluca weighed at first: at the end of 8 or
nine days the matter being look'd upon against the light was discern'd to
<send up>[replacing 'emit'] manifest
smoake[altered from 'smoke'] or
fumes, & even this night when it was stir'd with a small stick of Glass we
saw it
[ 'manifestly' deleted] Emit Fumes not only manifest but in proportion
to the body
[ 'Copious' deleted] that afforded them Copious.
[Integral marginalia:]
Sept. 17.
[Retrospective marginalia:]
5
We took a fragment of
Solid Noctiluca of about the bignesse of a
[ 'sm' deleted] pea, &
placing
it['ing it' inserted above 'd' deleted] between two flat pieces of clean glasse, endeavor'd for tryalls sake
to extinguish it, as men are wont to do bits of kindled charcoale, snuffs of
candles &
[ 'f' deleted] other such common fires by compression. But thô we
thrust the two pieces of glasse strong against one another yet we were not
[ 'by' deleted] able by this means to extinguish the fire, or
<totally> destroy the luminousnesse of the matter. for all
about the edges, the matter shone very near if not full as vivid
<ly> as before, & so it did over all the lower surface
too, when the glasse has been separated that surface enjoy'd the contact of the
air. But the upper part of this noctilucall matter, which because of the
pressure it had been expos'd to, stuck very close to the lower surface of this
upper glasse, & was thereby fenc'd from the contact of the Air Appear'd
black or considerably except as was lately noted at the edges which were
touch'd by the Air whether the two glasses were kept compresst, or the darken'd
part was lookt on through the upper glasse only.
[Integral marginalia:]
Sept. 19. 90
[Retrospective marginalia:]
6
[ 'Three' deleted] To make the {mercury}iall {water} for silvering over
{copper} wee ground together 3 parts of {sal ammoniac} to 2 of {mercury} &
{sublimate}d the mixture in a vessel then we tooke the
white part of the sublimate [BP 21, p. 247] & having separated
the little globules of running {mercury} that were yet dispers'd among it, we
dissolvd it in fair {water}, & by filtring the sol. thorough cape paper we had a limpid liquor fit to
give very clean {copper} the colour of {mercury} in a trice, this
sol. gave a white
<{precipitate} with oyl of {urine}> not a yellow one as common
{sublimate}te does; & so it did with sp.
<of> {urine}ne.
[Integral marginalia:]
oct. 3. 90
[Retrospective marginalia:]
7
About noone the weather being but indifferently clear & faire
the {sun} beams were suffered to fall upon a flate looking, & were
reflected thence so
[ '(' deleted]as to fall conveniently upon the greater dioptricall burning
glasse, which was plac't
<about> six foot from the
[ 'burning glasse' deleted] other, & the focus of the burning glasse
being made to fall upon a piece upon a piece of black paper
[ 'did' deleted] presently burnt a hole in it, & allso producd a good
deal of smoake in a piece of a wooden box blackt with Charcoal.
[Integral marginalia:]
Oct. 21. 90.
[Retrospective marginalia:]
8
48 grains
<- 1/4> of perfumed candle being kindled & suffer'd
to burn of it self did give 4 grains of Ashes that made no Alteration on syrop
of Violets.
[Integral marginalia:]
oct. 21.
[Retrospective marginalia:]
9
Two {ounce} of {sulphur} & one of {mercury} being mixd &
<kept>
stirring[altered from 'stirred'] over
the fire till the {sulphur} was wasted afforded {drachm} v
of Æthiops Niger of which powder many little particles were glittering.
[Integral marginalia:]
oct 25 90.
[Retrospective marginalia:]
10
The rectifyd sp. of fresh horse dung,
had no {urine}ous smell or tast, thô it were penetrative enough upon the
tongue. It had but a very faint acidity, & yet it was of an acid rather
then an alcalisate nature, the first appeard by this that its tast was not
[ 'manifestly' deleted] sensibly acid, it would not manifestly worke upon
powder'd corall, nor so much as make an undoubted conflict with {salt of tartar}
(& at least it did not in the small quantitys of both that we employ'd) but
yet it had some acidity appeard by its readily depriving the double {tincture}
of its blewnes, & by its as readily
[ 'pr' deleted] making a white {precipitate}tate
[ 'of' deleted] with the Red lixiviall
<solution or> {tincture} of {sulphur}.
[Integral marginalia:]
Nov. 5. 90
[Retrospective marginalia:]
11
The Rectifyd sp. of Hay drawn in a
retort did appear much more manifestly acid than the sp. of fresh horse-dung for it readily tooke away the
blew colour from the double {tincture}, or the red from the {tincture} of
Brasil it made syrop of violets purplish, & had the operation it should
have as an acid, on two or three other bodies.
Spirit of barly drawn in a retort & put to rectifye
<the more volatile part>[replacing 'a good portion'] of the liquor
<which was that,> that first came over seemd by the tast
& smell to consist mainly of an anonymous [BP 21, p. 248]
spirit, & yet not so entirely, but that by some of our ordinary ways of
tryall we concluded it to be acid. But the acidity was much more manifest in
the red liquor that remaind, & so was rather dephlegmd than rectifyd for
this liquor readily tooke off the rednes of a {tincture} of brasil, &
[ 'not only' deleted] made an audible as well as a visible ebullition
with {salt of tartar} but readily wrought briskly enough upon crude corall in the
cold.
[Integral marginalia:]
90
[Retrospective marginalia:]
12
The reddish sp. that came over with the vol. Salt of nettles (that shot in it into such fine
Chrystalls) as it smelt like an Animal sp. so like
an {urine}ous sp. it
[ 'pr' deleted] made with sol. of
sublimate a white precipitate, it restord blewness to the disanimated double
{tincture}, it turnd syrup of violetts green & made a great conflict &
frothy ebullition with {spirit} of {salt}.
[Retrospective marginalia:]
13
For severall purposes,
& particularly to make an alcalisation of {nitre} without charcoale, or
other such combustible bodies, we tooke {ounce} vi of fine
{nitre}, & as much burnt {alum}, & having mixt them we put them into an
open crucible, we kept that vessell & the contained matter,
<red hot> for above two houres, & then taking it out of
the crucible, it appear'd that we had lost five ounces of the first weight (or
twelve ounces) some of the matter at the bottome was found to have been melted
& to have acquired partly a yellowish, & partly a greenish blew colour,
the rest of the matter was white, & seem'd
<not> to be
[ 'let' deleted] much, thô it was a little alter'd but the lower
part manifested it self to be alcalisd by readily affording a yellow
{precipitate}tate with sol. of {sublimate} &
the turning of the Syrop of violets into a deep green.
[Retrospective marginalia:]
14
Fine white Borax destilld per se in a retort plac't in Sand afforded
a more copious liquor than we expected, which thô it was so very faintly
acid as to be allmost quite insipid & not to make any visible conflict with
salt of {tartar}, did yet appear not quite devoyd of acidity since it turnd the
syrop of violets purplish, & readily depriv'd the double {tincture} of its
blewnes.
[Retrospective marginalia:]
15
Equall parts of fine Borax & {oil} of {vitriol} being distilld
by degrees of fire, which was made so strong at last as to keep the retort two
or three hours red hot in [BP 21, p. 249] the Sand, afforded a good
quantity of a very corrosive liquor, & which may seem strange a
considerable proportion of salt that ascended with it & passd into the
receiver thô it was perceiv'd that the mixture
[ 'from' deleted] committed to destill sent up any white or red fumes,
like {nitre}, {salt}, {vitriol} &c. the {caput mortuum} was for the most
part turnd into a lump of fine glasse.
[Retrospective marginalia:]
16
Two {ounce} of Borax calcin'd in a glasse {retort}, & the like
weight of good burnt {alum}, were mixt & put into a crucible, where in a
fire not violent the
<mixture> puft, & swelld considerably & for a good
while, then twas kept about an houre, & a half in Fusion,
[ '& the' deleted] whereby the most part of it was brought into a
transparent & colourless glasse, as the rest that lay in a lump at the
bottome, would in all probability have been,
<if it> had been kept longer in the fire the crucible being
broken, a
[ 'good' deleted] part of the matter
<that was supposd to weigh three or four dragms> stuck
<too> close to the syds & bottom of it to be easily
recover'd
[ 'it' deleted] the weight of the glasse which was allmost all glasse
amounted to 10 grains.
[Retrospective marginalia:]
17
Sp. {verdigris}, in a moderate heat, did
draw a red {tincture} from glasse of Antimony made per
se in 36
[ 'how' deleted] howres.
[Retrospective marginalia:]
18
[ 'Wee too' deleted] Equall parts of {sal ammoniac} & Roch allome being
dissolv'd in fair water, & very slowly evaporated a good part of the allome
shot in grains figur'd as crystalls of that salt are wont to be long before any
of the {sal ammoniac} appear'd to shoote in its proper figure, namely of combs,
or of feathers.
[Integral marginalia:]
Dec. 25
[Retrospective marginalia:]
19
To show how much, even those that are calld first Qualityes depend
upon the Texture
[ '& Circumstances' deleted] of Agents, & patients, &
<mechanicall> Circumstances of action wee made the following
Experiment, which thô somewhat odde answer'd
my expectation. Upon
<two or three spoonfulls (by estimate) of
snow>[replacing 'a little'] snow put into a thin viall wee pour'd about half a
<spoonefull>[replacing 'spoone'] by guesse of
[ 'th' deleted] good oyle of {vitriol}
[ 'upon two or three spoonfulls (by estimate) of snow' deleted], &
having observd that the menstruum
[BP 21, p. 250] did, as it should
<do>, make a speedy solution of the snow, wee presently put the
bottome of the glasse that held the mixture into
water, where it produc'd as wee desir'd not only an actuall cold, but in the
[ 'con as' deleted] contiguous parts of the surrounding liquor, so intense
a one, that allmost as farre as the mixture reacht,
the outside of the glasse was cas'd over with Ice manifestly sticking
<to it>, & not without some difficulty to be scrapd of with
a knife, & this glaciation was performd in about a minuts tyme.
[ 'Afterw' deleted] Afterwards suffering the snow to be quite dissolvd, we
proceeded to the 2d part of the Experiment, which
was to poure out of the same viall, some fresh {oil} of {vitriol}, into the
fore-mentiond cold mixture, whereupon there presently
insud as we lookt for not only a manifest but a very considerable degree of
heat. This Experiment being repeated & succeeded
the 2d tyme
<with [approximately 5 characters illegible]>
with this difference, that when more oyle of vitrol was put into the dissolvd
& already impregnated Ice, the mixture grew so hot
that
<I found the
heat glasse too hot to
hold continue to hold it in my hand>[replacing 'it obligd me to']
[Retrospective marginalia:]
20
It may give light into the nature of Cold to know whether, or no, a
liquor environ'd by another may be turn'd into Ice,
[ 'what' deleted] thô the ambient liquor remaine unfrozen. To resolve
this enquiry we
<suspended>[replacing 'put'] a small round bubble almost full of common water in a vessell
containing sufficient quantity of
[ 'the' deleted] oyle of Turpentine. This vessell being encompassd with
<our> frigorik mixture of Ice &
{vitriol}, the water in the bubble was after some minutes found glaciated, the
ambient oyle continuing fluid.
Jan. 1. 90/91
[Retrospective marginalia:]
21
To
<confirme
what I the conjecture I elsewhere offer is>[replacing 'show'] that some winds may derive a great degree of coldnesse from
that of bodies over which, or through which they passe, wee tooke a seal'd,
& Gagd Thermometre, & having settled it in a fit posture, wee caus'd
the common Aire of my chamber to be blowne a while upon it, with a paire of
ordinary hand bellows by which
<means it was>[replacing 'it descended'] but a very little
<that it descended> then observing that the
<red>[replacing 'tincted'] {spirit of wine} rested at about a quarter of a division or Inch
below the mark
[ 'to whi' deleted] [BP 21, p. 251] which was set to denote
frost, wee encompasd a great part of the pipe of the same bellows, with beaten
Ice, & then blew upon the ball of the Thermoscope as before, & soon
perceivd the Spirit to subside (
<thô> not hastily) more & more till it came to be
about three quarters beneath three then to make the cold more keen we mixt the
Salt with the Ice that lay about the pipe & found as wee expected that the
liquor descended afresh & continu'd to do so for a while till it
[ 'a little ben 4th' deleted] it had fallen
<in all far
as>[replacing 'lower by another'] the 4th of a division from its first station
[Integral marginalia:]
Jan: 12 1690/91
[Retrospective marginalia:]
22
A green finch newly killd &
plumd was this day put entire to be preservd into a wide mouth glass coverd
with a flat plate of glass ground exquisitely to it at kept down by a spring to
make it continue close.
[Integral marginalia:]
Jan 30.
[Retrospective marginalia:]
23
Four ounces of {sulphur}
v. being powderd & put into a small, but not a
very small retort were put into a Sand capell
<fire>[replacing 'where'] was administred to it: for about 4 houres, being made very
strong toward the latter end of that tyme, the event was
<That>[replacing 'that'] there passd no liquor into the Receiver, that there sublim'd
into the neck of the Retort an ounce, & a dram, & about a half of pure
fine {sulphur} melted into a lump a good part of which appear'd allmost
transparent the Capaut Mortuum lookt prettily abounding with glittering
corpuscles, it weigh'd
[space of 13-15 characters]
[ 'b' deleted] but I cannot alltogether depend upon this weight because
I perceiv'd a crack in the glasse thô I did not discern that any thing
was run out of it.
[Retrospective marginalia:]
24
Four ounces of {sal ammoniac} & as much {lime} being (separately)
powder'd & mixt
[ 'b' deleted] were put by spoonfulls into a red hot crucible, & when
all the stuff was in it was melted with a strong fire & the matter
[ 'being pou' deleted] pour'd out was found to weigh about six ounces. the
glasse did break through the violence
[ '&' deleted] of the fire so that some of the matter was lost in the
sand.
[BP 21, p. 252]
[Retrospective marginalia:]
25
An ounce of strong {spirit} of
{salt} & as much {spirit} of {sal ammoniac} made with quicklime afforded a
little phlegmatic liquor & in the neck of the retort {drachm}
ii & about an half of {sal ammoniac} which lookt very
prettyly.
[Integral marginalia:]
feb. 6
[Retrospective marginalia:]
26
A pound of {mercury}
being kept in the Frigorifick mixture (of 4 parts of
Ice to 1 of {salt}) till it was allmost dissolv'd, the
<
[ 'Gagd' deleted]> Thermoscope
<with Amel>, that was before brought to
[ 'ad' deleted] the temper of the
<ambient> water by standing in it some tyme,
<at the end of which it rested 1/2 division
above the fourth black bead>[insertion in margin ] was, by putting into it this
<viall containing the> infrigidated {mercury}, made to
subside in a few minuts, 3/10 of
a['n' at end of word deleted]
division, & 1/2. The same Thermoscope after being reduc'd
<to the temperature> of more of the same water
<in another vessel>[replacing 'b'] as before, was by putting {oil} {vitriol}li about
[space of 6 characters] infrigated
[ 'as before' deleted], had its ting'd Sp.
brought down to 8/10 of a division,
[ 'from the so' deleted] one above, & 7 beneath the same black
<bead>, it subsyded more hastily than the {mercury} made it
do, & which is more the bottle being kept somewhat longer in the water,
appear'd to have gaind a piece of Ice thô not a thick one,
<stuck to>[replacing 'on'] the outsyde of the Glasse.
[Integral marginalia:]
feb. 27 90
[Retrospective marginalia:]
27
Half an ounce of good rectifyd butter of {antimony} being well washt
with water afforded {drachm} ii g. xxv of very white & somewhat glittering {mercury}
vitæ.
{sal ammoniac} & {lime} ana lb i
averd. being well powderd & melted together
did give lb i {ounce} ii {drachm}
vii of
[space of half a line]
[Integral marginalia:]
19.
[Retrospective marginalia:]
28
The Braisilian plant which is specifick for bloody fluxes is in
their language called Beguguill.
[Retrospective marginalia:]
29
Two pound of {sal ammoniac}, &
as much quicklime, being first melted, & then kept in fusion for half an
hour after afforded lb ii & above four ounces of
matter strongly cakd.
[ '30. This day was p' deleted]
March 25 1691
[Retrospective marginalia:]
30
This day was put up, as
much blood as was taken at one phlebotomy from a young man at the shop of a
French Surgeon where I had a bolt-head with a long neck & a funnel at which
the blood
[ 'w' deleted]as soon as 'twas taken out of the vein might be conveyd
hot, & uncoagulated into the vessell, which I caus'd presently to be closd
up stop, & set asyde in a quiet place to be there kept & have its
changes, if any shall happen, observ'd.
[BP 21, p. 253]
Wee tooke a Cylindrical Tube of glass
closed at one End
<&> open at the other into this wee pour'd common water
to the hight of one foot carefully measur'd then pouring out the water into
another glass & drying the tube on the inside, wee put into
[ 'f' deleted] it fine & dry wood Ashes
<
& lightly shook>[replacing 'till they did'] & lightly shook them
[ 'w' deleted] but without compressing them till they reach'd the above
mention'd hight mark'd
<with a graver> on the out side of the Pipe then wee pour'd
back
[ 'y' deleted] some of the foremention'd water & when that was
soaked
[ 'm' deleted] up more which
[ 'pier' deleted] pierced downwards slowly enough but at Length it
arriv'd at the bottome when all the water was pour'd in. The mixture being
suffer'd to settle for
[ 'at least a day' deleted] two or three days the ashes were found to
have subsided Little by little & the supernatant water was growne cleare.
[ 'then we measur' deleted] This done we measur'd the two bodys againe
& found that the water was three Inches &
<about>[replacing 's'] three quarters above the mark
<& about two Inches & a halfe beneath it> &
consequently the
[ 'foot of' deleted] Ashes that took up the space of a foot in the Tube
were
<not>[replacing 'not'] able to
[ 'containe mu' deleted] soak up
[ 'much above two two third of the' deleted] before they began to
subside much above two thirds of the Cylindricall foot of water & after
they were settled there swam near halfe an Inch more then halfe a foot above
them.
[ 'The same' deleted] An Experiment to the same purpose being tryed
with first puting in a Cylindricall foot of Ashes & when they were taken
out as much water as reached to the same hight the Ashes being by degrees put
in & Lightly shaken but not suffer'd to rest many hours made the water rise
three Inches & three Eights about the
[ 'mark that deg' deleted] formerly mention'd mark distant a foot from
the bottome of the Tube by all which it appears that the Vulgar Tradition that
a glass of Ashes will containe as much water as [BP 21, p. 254] tho
there were
[ 'any' deleted] not any Ashes in the Vessell is farr from being
true.
[Integral marginalia:]
Jun 10. 91.
A pound of {copper}
averd. weight being kept in the glasse house
d. 38 acquir'd 2 ounces & two dragms more of the
same weight.
{copper} plates which
<in>[replacing 'at'] the shop they were bought at weigh'd a lb averdupois weight,
being kept in the glasse house in a heat capable to keep
[ 'the' deleted] glasse in fusion for 38 days, app
Wee took {copper} plates cutt small which in the balance of the shop
they were bought in weigh'd a lb averdupois & left them to calcine at a
glasse in a heat capable of keeping glas melted at the end of 38 days we found
the plates calcin'd & brittle as if they had been calcind
[ 'with' deleted] by stratification with sulphur; & thô there
remaind a small lump guess'd to
<weigh>[replacing 'be'] about a dram that chancd to be left uncalcind yet the whole pound
of {copper}
[ 'appeard' deleted] being weighd in our balance appeard to have gaind
computing by estimate some fragments that were employd upon tryalls, or
casually lost about two ounces of averd.
weight.
[Integral marginalia:]
July. 23 91
[ '{ounce} ii {oil} {vitriol} & {ounce}
viii {drachm} vii
sp. {urine}
<which was enough> to satiate it, be' deleted]
{oil} {vitriol} {ounce} ii
[ '&' deleted] took {ounce} viii {drachm}
vii of good sp. {urine} to
satiate it, & being filtred & evaporate to a drynes gave a white {salt}
but brownish towards the bottome weighing {ounce} i
{drachm} vi g. LV.
[Integral marginalia:]
Aug. 91.
Wee mixed {ounce} xii of {sal ammoniac} &
{lime} ana first well powdered & sifted & set them to run
p. d.